{"title":"合成具有良好电化学性能的 BiDy 复合氧化物纳米片","authors":"Chenxu Feng, Qianmin Cong, Xiaoyu Wang, Jiayin Cui, Lizhai Pei","doi":"10.1680/jnaen.23.00066","DOIUrl":null,"url":null,"abstract":"BiDy composite oxide nanoflakes with the thickness of about 50 nm were synthesized by one-step hydrothermal method. The electrodes modified with BiDy composite oxide nanoflakes exhibit superior electrochemical behavior for detecting L-cysteine using cyclic voltammetry (CV) method. The impact of scan rate, electrolyte, and concentration of L-cysteine for electrochemical behaviors were investigated. A pair of strong quasi-reversible CV peaks are observed at +0.03 V (cvp1) and –0.69 V (cvp1′) with peak current of 171.2 μA and 171.3 μA, respectively for the BiDy composite oxide nanoflake-modified GCE in 0.1 M KCl and 2 mM L-cysteine solution. GCE modified with the BiDy composite oxide nanoflakes displays broad range of linearity (0.001-2 mM) and low detection limit (0.29 μM) for L-cysteine. Using a hydrothermal approach as a synthesis technique for nanoflakes, as well as a facile and sensitive electro-chemical sensor based the nanoflakes was developed to detect L-cysteine, makes it a promising approach for practical application.","PeriodicalId":44365,"journal":{"name":"Nanomaterials and Energy","volume":null,"pages":null},"PeriodicalIF":0.3000,"publicationDate":"2024-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis of BiDy composite oxide nanoflakes with good electrochemical properties\",\"authors\":\"Chenxu Feng, Qianmin Cong, Xiaoyu Wang, Jiayin Cui, Lizhai Pei\",\"doi\":\"10.1680/jnaen.23.00066\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"BiDy composite oxide nanoflakes with the thickness of about 50 nm were synthesized by one-step hydrothermal method. The electrodes modified with BiDy composite oxide nanoflakes exhibit superior electrochemical behavior for detecting L-cysteine using cyclic voltammetry (CV) method. The impact of scan rate, electrolyte, and concentration of L-cysteine for electrochemical behaviors were investigated. A pair of strong quasi-reversible CV peaks are observed at +0.03 V (cvp1) and –0.69 V (cvp1′) with peak current of 171.2 μA and 171.3 μA, respectively for the BiDy composite oxide nanoflake-modified GCE in 0.1 M KCl and 2 mM L-cysteine solution. GCE modified with the BiDy composite oxide nanoflakes displays broad range of linearity (0.001-2 mM) and low detection limit (0.29 μM) for L-cysteine. Using a hydrothermal approach as a synthesis technique for nanoflakes, as well as a facile and sensitive electro-chemical sensor based the nanoflakes was developed to detect L-cysteine, makes it a promising approach for practical application.\",\"PeriodicalId\":44365,\"journal\":{\"name\":\"Nanomaterials and Energy\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.3000,\"publicationDate\":\"2024-06-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Nanomaterials and Energy\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1680/jnaen.23.00066\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Nanomaterials and Energy","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1680/jnaen.23.00066","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Synthesis of BiDy composite oxide nanoflakes with good electrochemical properties
BiDy composite oxide nanoflakes with the thickness of about 50 nm were synthesized by one-step hydrothermal method. The electrodes modified with BiDy composite oxide nanoflakes exhibit superior electrochemical behavior for detecting L-cysteine using cyclic voltammetry (CV) method. The impact of scan rate, electrolyte, and concentration of L-cysteine for electrochemical behaviors were investigated. A pair of strong quasi-reversible CV peaks are observed at +0.03 V (cvp1) and –0.69 V (cvp1′) with peak current of 171.2 μA and 171.3 μA, respectively for the BiDy composite oxide nanoflake-modified GCE in 0.1 M KCl and 2 mM L-cysteine solution. GCE modified with the BiDy composite oxide nanoflakes displays broad range of linearity (0.001-2 mM) and low detection limit (0.29 μM) for L-cysteine. Using a hydrothermal approach as a synthesis technique for nanoflakes, as well as a facile and sensitive electro-chemical sensor based the nanoflakes was developed to detect L-cysteine, makes it a promising approach for practical application.