超声波振动辅助粉末混合电火花加工银整合技术用于抗菌表面

Viet D. Bui , André Martin , Thomas Berger , Karsten Harnisch , Joachim Döring , Jessica Bertrand , Andreas Schubert
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引用次数: 0

摘要

使用纳米银粉末的粉末混合放电加工(PMEDM)证明了其在抗菌表面改性方面的潜在能力。对横截面层的分析表明,银主要集成在最顶层的表层附近,其含量在表层内向基底方向减少。以往的研究表明,超声波振动(UV)辅助 PMEDM 可以使沉积层中的银含量均匀化。本研究探讨了紫外线对改性层内银分布的影响。Ti6Al4V 工件受到频率为 22.3 kHz、振幅为 2.5 µm 的紫外线刺激。以碳氢化合物为基础的介电流体与浓度高达 15 克/升的纳米银粉末混合后,以 4 巴的压力通过空心工具进行内部冲洗。作为对比,还研究了不含紫外线的 PMEDM。通过共聚焦显微镜、扫描电子显微镜和能量色散 X 射线光谱分析了沉积层厚度、微裂纹和沉积银的横截面分布。结果表明,使用紫外线可使银层中间区域的银含量最高,微裂纹显著减少,银层厚度略有降低。
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Ultrasonic Vibration assisted Silver Integration by Powder Mixed EDM for Antibacterial Surfaces

Powder mixed electrical discharge machining (PMEDM) with silver nano-powder has demonstrated its potential capability in antibacterial surface modification. Analyses in the cross-sectional layer showed that silver was mainly integrated near the topmost surface layer, and its content is reduced within the layer towards the substrate. However, to achieve a long-term antibacterial efficacy, silver needs to be deeply integrated in the modified layer.

Previous studies indicated that ultrasonic vibration (UV) assisted PMEDM can homogenize the silver content in the deposited layer. In this study, the effect of UV on the silver distribution within the modified layer is investigated. Ti6Al4V workpieces were stimulated by UV with a frequency of 22.3 kHz and an amplitude of 2.5 µm. Hydrocarbon-based dielectric fluid, mixed with silver nano-powder with concentrations up to 15 g/L, were internally flushed through a hollow tool with a pressure of 4 bar. PMEDM without UV was investigated for comparison. The layer thickness, micro-cracks and the cross-sectional distribution of deposited silver were analysed by confocal microscopy, scanning electron microscopy, and energy-dispersive X-ray spectroscopy. Results indicate that applying UV leads to the highest silver content in the middle region of the layer, a significant decrease of micro-cracks and a slight reduction of the layer thickness.

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