封装荧光标签用于标记钻屑,以改进深度相关性:现场应用

SPE Journal Pub Date : 2024-06-01 DOI:10.2118/221466-pa
S. S. Zhu, M. Antoniv, N. Saadoun, G. Thomas, M. Poitzsch, H. Kwak, A. Yousef
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引用次数: 0

摘要

钻屑录井(泥浆录井)是一项在地层评估和完井效率方面具有巨大潜力的技术。然而,传统的泥浆测井技术使用切削回程的滞后时间来确定切削样本深度,这导致深度不确定性达到±20 英尺或更高。我们之前曾提议在钻头面使用渗透浸渍聚合物纳米标签(NanoTags)标记切样,并利用纳米标签的下行时间确定切样深度,这样可将深度不确定性降至±1-2 英尺。在该测试中,使用热解气相色谱质谱分析法(Py-GC/MS)检测到了切屑中的 NanoTags 信号。该技术开发的第二次实地测试于 2022 年进行,使用的是封装罗丹明染料的新一代光学 NanoTags。我们还开发了一种检测方法,利用荧光显微镜和 ImageJ 软件对插条上的光学标签进行半定量分析。结果表明,我们的标签技术确定的深度是准确的,与泥浆测井数据相关性良好;结果还表明,每次标签注入之间的最佳间隔时间应大于 10 分钟。
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Encapsulated Fluorescent Tags to Label Drill Cuttings for Improved Depth Correlation: A Field Application
Drill cuttings logging (mud logging) is a technology with great potential to deliver formation evaluation and completion efficiency. However, the conventional mud logging technology determines the cutting sample depth using the lag time of the cutting’s return trip, which results in depth uncertainties of ±20 ft or more. We previously proposed to tag cuttings at the bit face with penetrating, impregnating polymeric NanoTags and to determine the cuttings’ depth using the NanoTag’s downward trip time, which could reduce the depth uncertainties to ±1–2 ft. The first field test to test the first generation of NanoTags was completed in December 2019. In that test, the signals of the NanoTags in the cuttings were detected using pyrolysis gas chromatography mass spectrometry (Py-GC/MS) analysis. The second field test for the development of this technology was performed in 2022 using a new generation of optical NanoTags that encapsulated a rhodamine dye. A detection method was also developed to analyze the optical tag on cuttings semiquantitatively using a fluorescent microscope and ImageJ software. Our results suggest that the depth determined by our tagging technology is accurate and correlates well with the mud logging data; the results also indicated that the optimal gap time between each tag injection should be greater than 10 minutes.
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