用燃烧法研究钴锌混合铁氧体的结构、介电和磁性

Q2 Physics and Astronomy Physics Open Pub Date : 2024-06-14 DOI:10.1016/j.physo.2024.100226
Banu S. Razikha , S.S. Mahesh , A. Manjunath
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引用次数: 0

摘要

利用自燃方法制备了掺杂 Zn+2 的钴铁氧体纳米粒子,其基本化学成分为 ZnxCo1-xFe2O4(x = 0 至 1:以 0.25 为单位)。通过 XRD 研究确认了拟议样品的相位。煅烧铁氧体的 XRD 图显示了单相尖晶石立方结构。在室温下,使用 HIOKI LCR 表(型号:3520-50)在 102 Hz-106 Hz 频率范围内进行了介电测量。在环境温度下,研究了合成纳米材料的介电常数(ε′)和介电损耗正切(tan δ)与频率和 Zn+2 浓度的函数关系,所有样品都表现出介电分散性。使用振动样品磁力计(VSM)在室温下对 ZnxCo1-xFe2O4 纳米铁氧体进行了磁性测量,CoZnFe2O4 体系的所有样品都表现出铁磁性。
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Structural, Dielectric and Magnetic studies of Mixed Ferrites of Co-Zn using combustion method

Using auto-combustion approach, cobalt ferrite nanoparticles doped with Zn+2 with the basic chemical composition ZnxCo1-xFe2O4 (x = 0 to 1: in steps of 0.25) were prepared. Phase confirmation of the proposed samples was confirmed through XRD studies. XRD pattern of the calcined ferrites revealed single phase spinel cubic structure. At room temperature, using HIOKI LCR meter (Model no: 3520-50) the dielectric measurements in the frequency range 102 Hz–106 Hz were performed. Dielectric constant (ε′) and dielectric loss tangent (tan δ) of synthesized nano-materials were investigated as a function of frequency and Zn+2 concentration at ambient temperature and all the samples exhibited dielectric dispersion. Magnetic measurements for ZnxCo1-xFe2O4 nano-ferrites were carried out at room temperature using a vibrating sample magnetometer (VSM), and all the samples of the system CoZnFe2O4 exhibited ferromagnetic behavior.

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来源期刊
Physics Open
Physics Open Physics and Astronomy-Physics and Astronomy (all)
CiteScore
3.20
自引率
0.00%
发文量
19
审稿时长
9 weeks
期刊最新文献
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