氧化物弥散强化钢中的氧化物颗粒在 Joyo 中子辐照下强度达到 158 dpa

IF 2.8 2区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Journal of Nuclear Materials Pub Date : 2024-06-24 DOI:10.1016/j.jnucmat.2024.155252
T. Toyama , T. Tanno , Y. Yano , K. Inoue , Y. Nagai , T. Ohtsuka , T. Miyazawa , M. Mitsuhara , H. Nakashima , M. Ohnuma , T. Kaito
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引用次数: 0

摘要

氧化物分散强化(ODS)钢是下一代反应堆的理想候选材料,我们研究了氧化物纳米颗粒在高温至高剂量中子辐照下的稳定性。日本原子能机构用 Joyo 对 14Cr-ODS 钢 MA957 进行了辐照,辐照条件分别为 502 ºC 时 130 dpa、589 ºC 时 154 dpa 和 709 ºC 时 158 dpa。对 ODS 钢中的氧化物颗粒进行了三维原子探针 (3D-AP) 和透射电子显微镜 (TEM) 观察,以确定其特征。在未辐照和辐照样品中都观察到了高密度的 Y-Ti-O 颗粒。在 502 ºC 时辐照至 130 dpa 和 589 ºC 时辐照至 154 dpa 的样品中,氧化物颗粒的形态(即平均直径、数量密度和化学成分)几乎没有变化。在 709 ºC 时辐照至 158 dpa 的样品中,数密度略有下降。任何经过辐照的样品的硬度与未经过辐照的样品相比几乎没有变化。结果表明,氧化物颗粒的存在是稳定的,即使在高达 700 ºC 的高温下受到 160 dpa 的高剂量中子辐照,材料的强度也能得到充分保持。
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Oxide particles in oxide dispersion strengthened steel neutron-irradiated up to 158 dpa at Joyo

We investigated the stability of oxide nano particles in oxide dispersion-strengthened (ODS) steel, which is a promising candidate material for next-generation reactors, under neutron irradiation at high temperature to high doses. MA957, a 14Cr-ODS steel, was irradiated with Joyo in Japan Atomic Energy Agency under irradiation conditions of 130 dpa at 502 ºC, 154 dpa at 589 ºC, and 158 dpa at 709 ºC. Three-dimensional atom probe (3D-AP) and transmission electron microscope (TEM) observation were performed to characterize the oxide particles in the ODS steels. A high number density of Y-Ti-O particle was observed in the unirradiated and irradiated samples. Almost no change in the morphology of the oxide particles, i.e. average diameter, number density, and chemical composition, has been observed in the samples irradiated to 130 dpa at 502 ºC and to 154 dpa at 589 ºC. A slight decrease in number density was observed in the sample irradiated to 158 dpa at 709 ºC. The hardness of any of the irradiated samples was almost unchanged from that of the unirradiated sample. It was revealed that the oxide particles existed stable, and the strength of the material was sufficiently maintained even after being neutron irradiated to high dose of ∼160 dpa at high temperature up to 700 ºC.

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来源期刊
Journal of Nuclear Materials
Journal of Nuclear Materials 工程技术-材料科学:综合
CiteScore
5.70
自引率
25.80%
发文量
601
审稿时长
63 days
期刊介绍: The Journal of Nuclear Materials publishes high quality papers in materials research for nuclear applications, primarily fission reactors, fusion reactors, and similar environments including radiation areas of charged particle accelerators. Both original research and critical review papers covering experimental, theoretical, and computational aspects of either fundamental or applied nature are welcome. The breadth of the field is such that a wide range of processes and properties in the field of materials science and engineering is of interest to the readership, spanning atom-scale processes, microstructures, thermodynamics, mechanical properties, physical properties, and corrosion, for example. Topics covered by JNM Fission reactor materials, including fuels, cladding, core structures, pressure vessels, coolant interactions with materials, moderator and control components, fission product behavior. Materials aspects of the entire fuel cycle. Materials aspects of the actinides and their compounds. Performance of nuclear waste materials; materials aspects of the immobilization of wastes. Fusion reactor materials, including first walls, blankets, insulators and magnets. Neutron and charged particle radiation effects in materials, including defects, transmutations, microstructures, phase changes and macroscopic properties. Interaction of plasmas, ion beams, electron beams and electromagnetic radiation with materials relevant to nuclear systems.
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