壳聚糖基复合材料对化学改性聚乳酸薄膜性能的影响

A. Grigorov, A. Viraneva, M. Marudova
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引用次数: 0

摘要

本文研究了在化学改性聚-D-乳酸(PDLA)表面制造壳聚糖基复合材料的问题。将聚对二乳酸(PDLA)溶解在氯仿中,然后浇铸到玻璃皿中,直至溶剂完全蒸发。用 1,6-己二胺和戊二醛对 PDLA 薄膜表面进行改性,以产生游离醛侧基。壳聚糖 (CH) 复合层沉积在改性薄膜的表面。使用测力计研究了复合薄膜的机械性能。使用扫描电子显微镜(SEM)研究了所制得的复合薄膜的表面形态。采用无水滴法测定了所制壳聚糖基复合膜的表面自由能。
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INFLUENCE OF CHITOSAN-BASED COMPOSITES ON THE PROPERTIES OF CHEMICALLY MODIFIED POLY-LACTIC ACID FILMS
The presented paper investigates the creation of chitosan-based composites on the surface of chemically modified poly-D-lactic acid (PDLA). PDLA was dissolved in chloroform and cast into a glass dish until the complete evaporation of the solvent. The surface of the created PDLA films was modified with 1,6-hexanediamine and glutaraldehyde for the creation of free aldehyde side groups. Composite layers of chitosan (CH) were deposited on the surface of the modified films. The mechanical properties of the composite films were investigated using a dynamometer. The surface morphology of the created composite films was studied with Scanning electron microscopy (SEM). Sessile drop method was used to determine the surface free energy of the created chitosan-based compositelayers.
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Journal of Chemical Technology and Metallurgy
Journal of Chemical Technology and Metallurgy Engineering-Industrial and Manufacturing Engineering
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