喷雾干燥法制备的奇异籽油微胶囊:优化与微胶囊特性

L. Cuevas-Glory, D.G. Rosel-Sosa, M.E. Ramirez-Ortiz, S. Gallegos-Tintoré, Y.A. Chim-Chi, L. Chel-Guerrero, D. Betancur-Ancona
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摘要

当前食品研究的一个趋势是开发有助于降低某些疾病风险的有益健康产品。奇异籽(Salvia hispanica L.)油是公认的必需脂肪酸(ω-3)来源,有助于预防心血管疾病。本研究对奇异籽油进行了表征,并对喷雾干燥过程前后的脂肪酸进行了鉴定。奇异籽油喷雾干燥实验采用了 32 因子设计和响应面方法。统计设计因素和水平如下:阿拉伯胶:麦芽糊精混合物(GA:MD)(1:1、1:2 和 1:3 w/w)和干燥温度(DT)(140、160 和 180°C)。在未加工的奇异籽油中发现了 67.9% 的不饱和脂肪酸,在微胶囊油中发现了 65.7% 的不饱和脂肪酸。喷雾干燥工艺的最佳参数如下:GA:MD 51:1,DT 180°C;粉末产出率 49.5%(w/w),颗粒平均大小 129 µm,球形系数 0.11。随着时间的推移,微胶囊有变质、变色和结块的趋势,从而降低了其流动能力。另一方面,该产品更易于处理,保护了油脂免受热量和湿气的影响,而且微胶囊工艺为油脂的活性物质(如欧米茄型脂肪酸)提供了稳定性。
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Chia seed oil microencapsulated by spray-drying: optimization and microcapsules characteristics
A current trend in food research is the development of beneficial health products that could help to decrease certain risks of diseases. The chia seed (Salvia hispanica L.) oil is a proven source of essential fatty acids (omega-3), which can help to prevent cardiovascular diseases. In this study, chia seed oil was characterized and fatty acids were identified before and after the spray-drying process. A 32 factorial design with response surface methodology was utilized for chia seed oil spray drying experiments. Statistic design factors and levels were as follows: gum arabic: maltodextrin mixture (GA:MD) (1:1, 1:2 and 1:3 w/w) and drying temperatures (DT) (140, 160, and 180°C). A total of 67.9% of unsaturated fatty acids were found in raw chia seed oil and 65.7% in microencapsulated oil. The optimal parameters for the spray drying process were as follows: GA:MD 51:1 and DT, 180°C; powder yield rate, 49.5% (w/w), mean size of particles 129 µm, and sphericity coefficient of 0.11. Microcapsules tended to demean over time, changing their color, and producing agglomerate, which decreased their flowing capacity. On the other hand, the product was easier to handle, the oil was protected from heat and moisture conditions, and the microencapsulation process provided stability to the oil's active substances, such as omega-type fatty acids.
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