利用电子反向散射衍射法测定β-钛合金中的α层取向。

IF 6.1 3区 材料科学 Q1 Biochemistry, Genetics and Molecular Biology Journal of Applied Crystallography Pub Date : 2024-06-27 eCollection Date: 2024-08-01 DOI:10.1107/S160057672400400X
Petr Harcuba, Jana Šmilauerová, Miloš Janeček, Jan Ilavský, Václav Holý
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引用次数: 0

摘要

研究了 Timetal LCB(钛-6.8 钼-4.5 铁-1.5 铝,重量百分比)的可蜕变β-钛基体中的α薄片的空间取向,并确定了α薄片中六方紧密堆积α晶格的取向。为此,结合使用了小角 X 射线散射、扫描电子显微镜和电子反向散射衍射等方法。α薄片的习性平面接近{111}β,相当于α相六方坐标系中的(1320)α。最长的α薄片方向大致沿着与特定习性平面平行的〈110〉β方向之一。考虑到 β 和 α 相在 Timetal LCB 中老化条件下的平均晶格参数,不仅可以在母体 β 相的立方坐标系中,还可以在 α 相的六方坐标系中,对 α 薄片的所有主轴线和面进行索引。
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Determination of α lamellae orientation in a β-Ti alloy using electron backscatter diffraction.

The spatial orientation of α lamellae in a metastable β-Ti matrix of Timetal LCB (Ti-6.8 Mo-4.5 Fe-1.5 Al in wt%) was examined and the orientation of the hexagonal close-packed α lattice in the α lamella was determined. For this purpose, a combination of methods of small-angle X-ray scattering, scanning electron microscopy and electron backscatter diffraction was used. The habit planes of α laths are close to {111}β, which corresponds to (1320)α in the hexagonal coordinate system of the α phase. The longest α lamella direction lies approximately along one of the 〈110〉β directions which are parallel to the specific habit plane. Taking into account the average lattice parameters of the β and α phases in aged conditions in Timetal LCB, it was possible to index all main axes and faces of an α lath not only in the cubic coordinate system of the parent β phase but also in the hexagonal system of the α phase.

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来源期刊
CiteScore
10.00
自引率
3.30%
发文量
178
审稿时长
4.7 months
期刊介绍: Many research topics in condensed matter research, materials science and the life sciences make use of crystallographic methods to study crystalline and non-crystalline matter with neutrons, X-rays and electrons. Articles published in the Journal of Applied Crystallography focus on these methods and their use in identifying structural and diffusion-controlled phase transformations, structure-property relationships, structural changes of defects, interfaces and surfaces, etc. Developments of instrumentation and crystallographic apparatus, theory and interpretation, numerical analysis and other related subjects are also covered. The journal is the primary place where crystallographic computer program information is published.
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