高填充可流动树脂复合材料的挠曲性能、耐磨性和微结构分析

IF 1.4 4区 医学 Q3 DENTISTRY, ORAL SURGERY & MEDICINE Operative dentistry Pub Date : 2024-09-01 DOI:10.2341/24-033-L
P Francois, J P Attal, T Fasham, M Troizier-Cheyne, H Gouze, S Abdel-Gawad, S Le Goff, E Dursun, R Ceinos
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引用次数: 0

摘要

研究目的本研究旨在评估九种高填充可流动树脂复合材料相对于粘性和传统低填充可流动复合材料的弯曲性能和双体耐磨性。此外,还对微观结构进行了扫描电子显微镜(SEM)分析:对于每组树脂复合材料(n=12),使用硅模具制作 12 个试样棒(25 mm × 2 mm × 2 mm),用于进行抗弯强度(FS)、抗弯模量(E)、抗弯韧度(FT)、威布尔模量(m)测试和扫描电镜微观结构分析。每组有十根钢筋在万能试验机上进行三点弯曲试验,另外两根钢筋嵌入丙烯酸树脂中,然后用扫描电镜观察进行结构分析。在使用咀嚼模拟器进行的双体磨损测试中,每组树脂复合材料的 8 个试样(12 组,n=8)都是在特定模具中制造的,并对硬质合金球进行了 120,000 次循环磨损,并测量了深度损失。通过三次单因素方差分析和 Tukey 后检验,比较了不同组之间的弯曲和磨损性能:结果:本研究中测试的大多数高填充复合材料都表现出与粘性复合材料相似的抗弯强度(105.68 兆帕至 135.49 兆帕)和优异的耐磨性。这些复合材料的弯曲模量(介于 5.12 GPa 和 9.62 GPa 之间)介于本研究测试的粘性复合材料和低填充复合材料之间:本研究中测试的高填充可流动复合材料表现出不同的体外特性,但往往优于粘性树脂复合材料,这表明它们可用于后牙修复。
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Flexural Properties, Wear Resistance, and Microstructural Analysis of Highly Filled Flowable Resin Composites.

Objective: This study aimed to evaluate the flexural properties and two-body wear resistance of nine highly filled flowable resin composites relative to those of viscous and conventional low-filled flowable composites. In addition, scanning electron microscopy (SEM) analysis of the microstructures was performed.

Methods and materials: For each resin composite group (n=12), 12 specimen bars (25 mm × 2 mm × 2 mm) were fabricated using a silicon mold for performing flexural strength (FS), flexural modulus (E), flexural toughness (FT), Weibull modulus (m) tests, and SEM microstructural analysis. For each group, ten bars were tested using a three-point flexural test on a universal testing machine, while the other two were embedded in acrylic resin before being observed by SEM for structural analysis. During the two-body wear test with a chewing simulator, 8 specimens (12 groups, n=8) of each resin composite group were manufactured in a specific mold and subjected to 120,000 cycles of wear against a steatite ball, and the depth loss was measured. Three one-way ANOVA tests followed by Tukey's post hoc tests were conducted to compare the flexural and wear properties among the different groups.

Results: The majority of highly filled composites tested in this study exhibited similar flexural strengths (between 105.68 MPa and 135.49 MPa) and superior wear resistance to those of viscous composites. The flexural moduli (between 5.12 GPa and 9.62 GPa) of these composites were in between those of the viscous and low-filled composites tested in this study.

Conclusions: The highly filled flowable composites tested in this study exhibited different in vitro properties but were often superior to those of viscous resin composite suggesting their possible use for posterior restorations.

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来源期刊
Operative dentistry
Operative dentistry 医学-牙科与口腔外科
CiteScore
4.00
自引率
9.10%
发文量
124
审稿时长
6-12 weeks
期刊介绍: Operative Dentistry is a refereed, international journal published bi-monthly and distributed to subscribers in over 50 countries. In 2012, we printed 84 articles (672 pages). Papers were submitted by authors from 45 countries, in the categories of Clinical Research, Laboratory Research, Clinical Techniques/Case Presentations and Invited Papers, as well as Editorials and Abstracts. One of the strong points of our journal is that our current publication time for accepted manuscripts is 4 to 6 months from the date of submission. Clinical Techniques/Case Presentations have a very quick turnaround time, which allows for very rapid publication of clinical based concepts. We also provide color for those papers that would benefit from its use. The journal does not accept any advertising but you will find postings for faculty positions. Additionally, the journal also does not rent, sell or otherwise allow its subscriber list to be used by any other entity
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