利用三叶茄根提取物绿色合成银和铜纳米粒子及其特性比较研究

IF 0.8 4区 化学 Q4 CHEMISTRY, ORGANIC Russian Journal of Organic Chemistry Pub Date : 2024-10-14 DOI:10.1134/S1070428024070182
C. Sivakumar, M. Senthilkumar, G. N. Kousalya
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引用次数: 0

摘要

利用三叶茄根提取物作为封端代表,绿色合成银和铜纳米粒子。这些研究的目的是利用三叶茄根提取物合成纳米颗粒,为两种特殊金属(硝酸银和硫酸铜)作画。我们对合成的银纳米粒子和铜纳米粒子进行了比较研究,分别称取约 10 克的三叶茄根,将其转移到装有 100 毫升蒸馏水的 250 毫升烧杯中,煮沸约 25 分钟,然后过滤溶液,得到透明的提取物。将 10 毫升三叶茄根提取物滴加到 10 毫升硝酸银和硫酸铜溶液中(比例为 1:1),提取物用于还原 Ag+ 和 Cu2+ 离子。紫外可见光谱是一种常用技术。波长在 300-800 纳米之间的光通常用于表征尺寸范围在 2-100 纳米之间的五彩精华纳米粒子。分光光度吸收测量的波长范围分别为 400-450 纳米和 500-550 纳米,用于表征银纳米粒子和铜纳米粒子。傅立叶变换红外光谱法可用于表征表面化学性质。利用傅立叶变换红外光谱可检测附着在纳米粒子表面的有机官能团(羰基、羟基)和其他表面化学残留物。扫描电子显微镜和透射电子显微镜可用于纳米到微米尺度的形态表征。透射电子显微镜的分辨率是扫描电子显微镜的 1000 倍。
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Green Synthesized Silver and Copper Nanoparticles Using Solanum trilobatum Root Extract and Comparative Study of Characterization

The green synthesis of silver and copper nanoparticles using Solanum trilobatum root extract as a capping representative. These studies changed into excited up at the synthesis of nanoparticles to offer paintings for two exclusive metals (silver nitrate and copper sulfate) with the aid of using the use of Solanum trilobatum root. We did a comparative study of synthesized silver and copper nanoparticles using about 10 g of Solanum trilobatum root was weighed separately and transferred into 250 mL beakers containing 100 mL distilled water and boiled for about 25 min solutions were then filtered to get clear extracts. The extract was taken for the reduction of Ag+ and Cu2+ ions, and 10 mL of Solanum trilobatum root extract was added drop wise to 10 mL of silver nitrate and copper sulfate solution (1 : 1 ratio). The UV-visible spectroscopy is a commonly used technique. Light wavelengths in the 300–800 nm are generally used for characterizing colorful essence nanoparticles in the size range of 2 to 100 nm. Spectrophotometric absorption measurements in the wavelength ranges of 400–450 and 500–550 nm are used in characterizing the silver and copper nanoparticles, respectively. FT-IR spectroscopy is useful for characterizing surface chemistry. Organic functional groups (carbonyls, hydroxyls) attached to the face of nanoparticles and the other face chemical remainders are detected using FT-IR. Scanning electron microscope and transmission electron microscopy are used for morphological characterization at the nanometer to micrometer scale. Transmission electron microscopy has a 1000-fold higher resolution compared with scanning electron microscope.

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来源期刊
CiteScore
1.40
自引率
25.00%
发文量
139
审稿时长
3-6 weeks
期刊介绍: Russian Journal of Organic Chemistry is an international peer reviewed journal that covers all aspects of modern organic chemistry including organic synthesis, theoretical organic chemistry, structure and mechanism, and the application of organometallic compounds in organic synthesis.
期刊最新文献
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