在较高工艺温度下通过高效挤压制备的中等强度和高延展性 VW93A 镁合金型材的显微组织和变形行为

IF 5.8 2区 材料科学 Q2 CHEMISTRY, PHYSICAL Journal of Alloys and Compounds Pub Date : 2024-10-29 DOI:10.1016/j.jallcom.2024.177298
Shu Chang Li, Xingmao Mu, Xiang Dong Wang, Xi Zhao, Hong Bin Liu, Hai Long Liu
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The extruded profile featured a typical heterogeneous microstructure, composed of basal oriented deformed grains (~20%) enriched with needle-like γ'/long period stacking ordered (LPSO) phases, and diverse oriented dynamically recrystallized (DRXed) grains interspersed with sparse lamellar LPSO phases. Quasi in-situ EBSD analysis further revealed that excellent plasticity of alloy was primarily borne by diverse oriented DRXed grains, governed by early-stage basal &lt;a&gt; slip and sustained &lt;c+a&gt; slip and multiple slip proliferation. Besides, the differential deformation between coarse and fine grains promoted the formation of heterogeneous interfaces with higher geometrically necessary dislocation (GND) density, imparting additional hetero-deformation induced (HDI) hardening for the alloy. Unlike the strong heterogeneous interfaces between dissimilar materials, however, the soft heterogeneous interface between coarse and fine grains could also significantly coordinate deformation through strong multiple slip within coarse grains at high strain level, restricting cracks initialization at the interface. Finally, the study found that significant activation of non-prismatic slip and the phase stimulating nucleation (PSN)/pinning effect of bulk/strip LPSO phases under extrusion jointly promoted the formation of an abnormal (0001) texture. 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引用次数: 0

摘要

低温变形是制备高强度镁-钆-钇-锌-锆合金的主流方法,但它会影响变形条件和工艺效率。本研究报告介绍了 U 形 VW93A(Mg-8.8Gd-2.8Y-1.8Zn-0.5Zr)镁合金型材的制备方法,通过在安全工艺温度(480 ℃)下进行高效挤压,然后快速冷却(抑制动态析出的步骤),实现了强度和延展性的平衡。该型材的拉伸屈服强度(TYS)为 287 兆帕,挤压后的超常伸长率(EL)为 18.5%。老化后,TYS 进一步提高到 387 兆帕,EL 下降到 11.2%。挤压型材具有典型的异质微观结构,由富含针状γ'/长周期堆积有序(LPSO)相的基底取向变形晶粒(约 20%)和夹杂着稀疏片状 LPSO 相的多样化取向动态再结晶(DRXed)晶粒组成。准原位 EBSD 分析进一步表明,合金的优异塑性主要由不同取向的 DRXed 晶粒承担,受早期基底滑移、持续滑移和多滑移扩散的支配。此外,粗晶粒和细晶粒之间的不同变形促进了具有较高几何必要位错(GND)密度的异质界面的形成,为合金带来了额外的异质变形诱导硬化(HDI)。然而,与异种材料之间的强异质界面不同,粗晶粒和细晶粒之间的软异质界面也能在高应变水平下通过粗晶粒内部的强多重滑移显著协调变形,限制界面处的裂纹初始化。最后,研究发现在挤压作用下,非棱镜滑移的显著激活和块状/条状 LPSO 相的相刺激成核(PSN)/纺丝效应共同促进了异常(0001)纹理的形成。在拉伸加载过程中,具有(0001)纹理的晶粒表现出相对缓慢的{̅101̅101̅2}孪晶扩展和协同多滑移激活,从而增强了超屈服阶段的持续应变硬化。
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Microstructure and deformation behavior of medium strength and high ductile VW93A Mg alloy profile prepared by high-efficiency extrusion at a higher process temperature
Deformation at lower temperatures is the mainstream method for preparing high-strength Mg-Gd-Y-Zn-Zr alloys, but it compromises both deformation conditions and process efficiency. This study reports the preparation of a U-shaped VW93A (Mg-8.8Gd-2.8Y-1.8Zn-0.5Zr) Mg profile, achieving a balance of strength and ductility through high-efficiency extrusion at a safe process temperature (480 °C), followed by rapid cooling (a step to suppress dynamic precipitation). The profile exhibited a tensile yield strength (TYS) of 287 MPa with an exceptional elongation (EL) of 18.5% after extrusion. Upon aging, the TYS further increased to 387 MPa, with a sacrifice in EL to 11.2%. The extruded profile featured a typical heterogeneous microstructure, composed of basal oriented deformed grains (~20%) enriched with needle-like γ'/long period stacking ordered (LPSO) phases, and diverse oriented dynamically recrystallized (DRXed) grains interspersed with sparse lamellar LPSO phases. Quasi in-situ EBSD analysis further revealed that excellent plasticity of alloy was primarily borne by diverse oriented DRXed grains, governed by early-stage basal <a> slip and sustained <c+a> slip and multiple slip proliferation. Besides, the differential deformation between coarse and fine grains promoted the formation of heterogeneous interfaces with higher geometrically necessary dislocation (GND) density, imparting additional hetero-deformation induced (HDI) hardening for the alloy. Unlike the strong heterogeneous interfaces between dissimilar materials, however, the soft heterogeneous interface between coarse and fine grains could also significantly coordinate deformation through strong multiple slip within coarse grains at high strain level, restricting cracks initialization at the interface. Finally, the study found that significant activation of non-prismatic slip and the phase stimulating nucleation (PSN)/pinning effect of bulk/strip LPSO phases under extrusion jointly promoted the formation of an abnormal (0001) texture. During tensile loading, grains with (0001) texture exhibited relatively slow {101̅2} twinning propagation and synergistic multipleslip activation, enhancing the sustained strain hardening during the over yield stage.
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来源期刊
Journal of Alloys and Compounds
Journal of Alloys and Compounds 工程技术-材料科学:综合
CiteScore
11.10
自引率
14.50%
发文量
5146
审稿时长
67 days
期刊介绍: The Journal of Alloys and Compounds is intended to serve as an international medium for the publication of work on solid materials comprising compounds as well as alloys. Its great strength lies in the diversity of discipline which it encompasses, drawing together results from materials science, solid-state chemistry and physics.
期刊最新文献
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