快速:一个用于标引立方材料的电子衍射区轴斑图案的ImageJ宏。

IF 6.1 3区 材料科学 Q1 Biochemistry, Genetics and Molecular Biology Journal of Applied Crystallography Pub Date : 2024-11-26 eCollection Date: 2024-12-01 DOI:10.1107/S1600576724010215
Thomas E Weirich
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引用次数: 0

摘要

作为先前工作的扩展,ImageJ宏脚本RAPID(比率法模式索引)已经开发出来,允许使用Rn比率原理对校准和未校准区轴对齐的立方晶格电子衍射模式进行即时索引。该程序可用于索引区轴对齐的选定区域电子衍射模式,纳米束电子衍射模式,透射电子显微镜(TEM)菊池模式,甚至高分辨率(扫描)TEM图像的快速傅立叶变换。该程序允许用户通过调整边界参数和允许的晶格索引误差,快速评估所研究的材料是否属于立方晶体系统,是伪立方还是根本不是立方。该软件还允许人们区分某些区域轴方向的P, I和F Bravais格。对于校准的衍射模式,可以获得晶格参数,允许在结构数据库中验证所研究的材料或相识别。此外,该程序可用于测定或验证使用的仪器的相机常数时,参考物质的使用。因此,它是TEM实验室现场晶体分析的方便工具。
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RAPID: an ImageJ macro for indexing electron diffraction zone axis spot patterns of cubic materials.

As an extension to previous work, the ImageJ macro script RAPID (ratio-method pattern indexing) has been developed to allow instant indexing of calibrated and uncalibrated zone axis aligned electron diffraction patterns of cubic lattices using the Rn ratio principle. The program can be used to index zone axis aligned selected-area electron diffraction patterns, nanobeam electron diffraction patterns, transmission electron microscopy (TEM) Kikuchi patterns and even fast Fourier transforms of high-resolution (scanning) TEM images. The program allows the user to quickly assess whether the material under investigation belongs to the cubic crystal system, is pseudo-cubic or is not cubic at all by adjusting the boundary parameters and allowed errors for lattice indexing. The software also allows one to distinguish between the P, I and F Bravais lattices for certain zone axis directions. For calibrated diffraction patterns, the lattice parameters can be obtained, allowing verification of the material under investigation or phase identification in connection with a structural database. In addition, the program can be employed for determination or verification of the used instrument's camera constant when reference materials are used. Therefore, it is a convenient tool for on-site crystallographic analysis in TEM laboratories.

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来源期刊
CiteScore
10.00
自引率
3.30%
发文量
178
审稿时长
4.7 months
期刊介绍: Many research topics in condensed matter research, materials science and the life sciences make use of crystallographic methods to study crystalline and non-crystalline matter with neutrons, X-rays and electrons. Articles published in the Journal of Applied Crystallography focus on these methods and their use in identifying structural and diffusion-controlled phase transformations, structure-property relationships, structural changes of defects, interfaces and surfaces, etc. Developments of instrumentation and crystallographic apparatus, theory and interpretation, numerical analysis and other related subjects are also covered. The journal is the primary place where crystallographic computer program information is published.
期刊最新文献
Thermal diffuse scattering analysis of Ag2O binary system via X-ray powder diffraction. Top dusted adhesive tape sample preparation method for the X-ray diffraction analysis of small powder sample volumes with the Bragg-Brentano setup. Journal of Applied Crystallography welcomes eight new Co-editors. A new technical solution to the problem of increasing the resolution of X-ray diffraction methods. An extended thermal pressure equation of state for sodium fluoride.
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