{"title":"同步加速器粉末数据中的Sn(SO4)2·2H2O。","authors":"Øystein Slagtern Fjellvåg, Helmer Fjellvåg","doi":"10.1107/S2414314624011799","DOIUrl":null,"url":null,"abstract":"<p><p>Tin(IV) sulfate dihydrate, Sn(SO<sub>4</sub>)<sub>2</sub>·2H<sub>2</sub>O, was prepared in a reflux of sulfuric acid under oxidizing conditions. Its crystal structure was determined from powder synchrotron X-ray diffraction data and is constructed of (100) layers of [SnO<sub>4</sub>(H<sub>2</sub>O)<sub>2</sub>] octa-hedra (point group symmetry 1) corner-connected by sulfate tetra-hedra. Hydrogen bonds of moderate strength between the water mol-ecules and sulfate O atoms hold the layers together.</p>","PeriodicalId":94324,"journal":{"name":"IUCrData","volume":"9 Pt 12","pages":"x241179"},"PeriodicalIF":0.0000,"publicationDate":"2024-12-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11701753/pdf/","citationCount":"0","resultStr":"{\"title\":\"Sn(SO<sub>4</sub>)<sub>2</sub>·2H<sub>2</sub>O from synchrotron powder data.\",\"authors\":\"Øystein Slagtern Fjellvåg, Helmer Fjellvåg\",\"doi\":\"10.1107/S2414314624011799\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><p>Tin(IV) sulfate dihydrate, Sn(SO<sub>4</sub>)<sub>2</sub>·2H<sub>2</sub>O, was prepared in a reflux of sulfuric acid under oxidizing conditions. Its crystal structure was determined from powder synchrotron X-ray diffraction data and is constructed of (100) layers of [SnO<sub>4</sub>(H<sub>2</sub>O)<sub>2</sub>] octa-hedra (point group symmetry 1) corner-connected by sulfate tetra-hedra. Hydrogen bonds of moderate strength between the water mol-ecules and sulfate O atoms hold the layers together.</p>\",\"PeriodicalId\":94324,\"journal\":{\"name\":\"IUCrData\",\"volume\":\"9 Pt 12\",\"pages\":\"x241179\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2024-12-10\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11701753/pdf/\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"IUCrData\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1107/S2414314624011799\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"2024/12/1 0:00:00\",\"PubModel\":\"eCollection\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"IUCrData","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1107/S2414314624011799","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2024/12/1 0:00:00","PubModel":"eCollection","JCR":"","JCRName":"","Score":null,"Total":0}
Tin(IV) sulfate dihydrate, Sn(SO4)2·2H2O, was prepared in a reflux of sulfuric acid under oxidizing conditions. Its crystal structure was determined from powder synchrotron X-ray diffraction data and is constructed of (100) layers of [SnO4(H2O)2] octa-hedra (point group symmetry 1) corner-connected by sulfate tetra-hedra. Hydrogen bonds of moderate strength between the water mol-ecules and sulfate O atoms hold the layers together.
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