酒石酸介导溶胶-凝胶法制备多晶InGaZnO4

IF 0.3 Q4 METALLURGY & METALLURGICAL ENGINEERING Russian Metallurgy (Metally) Pub Date : 2025-01-23 DOI:10.1134/S0036029524701969
G. M. Zirnik, S. A. Sozykin, D. A. Uchaev, A. S. Chernukha, I. A. Solizoda, S. A. Gudkova, D. A. Vinnik
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引用次数: 0

摘要

摘要以酒石酸为有机络合剂,采用溶胶-凝胶法制备了三元氧化铟镓锌。用x射线衍射、透射电镜和扫描电镜对合成的样品进行了检测。总结这些研究方法的一致结果,我们可以得出,合成样品的颗粒大小取决于合成温度:合成温度最低时形成纳米颗粒团块,900℃烧结后检测到微米级颗粒。样品的结晶度随合成温度的升高而升高。所有样品都没有杂质结晶相,并且在样品体积上表现出均匀的铟、镓和锌分布。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

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Preparation and Synthesis of Polycrystalline InGaZnO4 via Tartaric Acid Mediated Sol–Gel Method

Abstract—A sol–gel method is developed to synthesize ternary indium–gallium–zinc oxide using tartaric acid as an organic complexing agent. The synthesized samples were examined by X-ray diffraction and transmission and scanning electron microscopy. Summarizing the consistent results of these research methods, we can state that the sizes of the particles composing the synthesized samples depend on the synthesis temperature: agglomerates of nanoparticles form at the lowest of synthesis temperatures, and micron-sized particles are detected after sintering at 900°C. The crystallinity of the samples increases with the synthesis temperature. All samples have no impurity crystalline phases and exhibit a uniform indium, gallium and zinc distribution over the sample volume.

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来源期刊
Russian Metallurgy (Metally)
Russian Metallurgy (Metally) METALLURGY & METALLURGICAL ENGINEERING-
CiteScore
0.70
自引率
25.00%
发文量
140
期刊介绍: Russian Metallurgy (Metally)  publishes results of original experimental and theoretical research in the form of reviews and regular articles devoted to topical problems of metallurgy, physical metallurgy, and treatment of ferrous, nonferrous, rare, and other metals and alloys, intermetallic compounds, and metallic composite materials. The journal focuses on physicochemical properties of metallurgical materials (ores, slags, matters, and melts of metals and alloys); physicochemical processes (thermodynamics and kinetics of pyrometallurgical, hydrometallurgical, electrochemical, and other processes); theoretical metallurgy; metal forming; thermoplastic and thermochemical treatment; computation and experimental determination of phase diagrams and thermokinetic diagrams; mechanisms and kinetics of phase transitions in metallic materials; relations between the chemical composition, phase and structural states of materials and their physicochemical and service properties; interaction between metallic materials and external media; and effects of radiation on these materials.
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