基于915 MHz固态微波源烧结氧化物陶瓷的烧结锻造新工艺

IF 6.2 2区 材料科学 Q1 MATERIALS SCIENCE, CERAMICS Journal of The European Ceramic Society Pub Date : 2025-07-01 Epub Date: 2025-02-04 DOI:10.1016/j.jeurceramsoc.2025.117262
Guillaume Rayrat , Alexis Onfroy , Christelle Bilot , Frédéric Bernard , Sébastien Lemonnier , Fabian Delorme , Charles Manière , Christelle Harnois , Sylvain Marinel
{"title":"基于915 MHz固态微波源烧结氧化物陶瓷的烧结锻造新工艺","authors":"Guillaume Rayrat ,&nbsp;Alexis Onfroy ,&nbsp;Christelle Bilot ,&nbsp;Frédéric Bernard ,&nbsp;Sébastien Lemonnier ,&nbsp;Fabian Delorme ,&nbsp;Charles Manière ,&nbsp;Christelle Harnois ,&nbsp;Sylvain Marinel","doi":"10.1016/j.jeurceramsoc.2025.117262","DOIUrl":null,"url":null,"abstract":"<div><div>This study presents the development of a fully instrumented sinter-forging process using a 915 MHz solid-state microwave source for the rapid and controlled sintering of dense oxide ceramics. Compared to conventional magnetron-based systems, the solid-state microwave source enables precise frequency tuning for optimal impedance matching and resonance conditions. Modeling and experimental characterization of the microwave applicator have enabled us to position the sample correctly in the cavity, ensuring efficient energy transfer and homogeneous heating. Sintering experiments carried out on alumina powder, both with and without applied pressure, revealed that the pressure-assisted process significantly improved densification, yielding near-complete density and increased hardness (21.6 GPa), while maintaining fine microstructures. This method highlights the potential of microwave-assisted sinter-forging for producing advanced ceramics with improved properties.</div></div>","PeriodicalId":17408,"journal":{"name":"Journal of The European Ceramic Society","volume":"45 7","pages":"Article 117262"},"PeriodicalIF":6.2000,"publicationDate":"2025-07-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"A new sinter-forging process based on a 915 MHz solid-state microwave source for sintering of oxides ceramics\",\"authors\":\"Guillaume Rayrat ,&nbsp;Alexis Onfroy ,&nbsp;Christelle Bilot ,&nbsp;Frédéric Bernard ,&nbsp;Sébastien Lemonnier ,&nbsp;Fabian Delorme ,&nbsp;Charles Manière ,&nbsp;Christelle Harnois ,&nbsp;Sylvain Marinel\",\"doi\":\"10.1016/j.jeurceramsoc.2025.117262\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>This study presents the development of a fully instrumented sinter-forging process using a 915 MHz solid-state microwave source for the rapid and controlled sintering of dense oxide ceramics. Compared to conventional magnetron-based systems, the solid-state microwave source enables precise frequency tuning for optimal impedance matching and resonance conditions. Modeling and experimental characterization of the microwave applicator have enabled us to position the sample correctly in the cavity, ensuring efficient energy transfer and homogeneous heating. Sintering experiments carried out on alumina powder, both with and without applied pressure, revealed that the pressure-assisted process significantly improved densification, yielding near-complete density and increased hardness (21.6 GPa), while maintaining fine microstructures. This method highlights the potential of microwave-assisted sinter-forging for producing advanced ceramics with improved properties.</div></div>\",\"PeriodicalId\":17408,\"journal\":{\"name\":\"Journal of The European Ceramic Society\",\"volume\":\"45 7\",\"pages\":\"Article 117262\"},\"PeriodicalIF\":6.2000,\"publicationDate\":\"2025-07-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of The European Ceramic Society\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0955221925000822\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"2025/2/4 0:00:00\",\"PubModel\":\"Epub\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, CERAMICS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of The European Ceramic Society","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0955221925000822","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2025/2/4 0:00:00","PubModel":"Epub","JCR":"Q1","JCRName":"MATERIALS SCIENCE, CERAMICS","Score":null,"Total":0}
引用次数: 0

摘要

本研究提出了一种采用915 MHz固态微波源的全仪器化烧结锻造工艺,用于致密氧化物陶瓷的快速可控烧结。与传统的基于磁控管的系统相比,固态微波源可以精确地调谐频率,以实现最佳的阻抗匹配和谐振条件。微波应用器的建模和实验表征使我们能够在腔中正确定位样品,确保有效的能量传递和均匀的加热。对氧化铝粉末进行了有压力和无压力的烧结实验,结果表明,压力辅助工艺显著改善了致密化,获得了接近完全的密度和硬度(21.6 GPa),同时保持了良好的微观结构。这种方法突出了微波辅助烧结锻造技术在生产具有改进性能的高级陶瓷方面的潜力。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
A new sinter-forging process based on a 915 MHz solid-state microwave source for sintering of oxides ceramics
This study presents the development of a fully instrumented sinter-forging process using a 915 MHz solid-state microwave source for the rapid and controlled sintering of dense oxide ceramics. Compared to conventional magnetron-based systems, the solid-state microwave source enables precise frequency tuning for optimal impedance matching and resonance conditions. Modeling and experimental characterization of the microwave applicator have enabled us to position the sample correctly in the cavity, ensuring efficient energy transfer and homogeneous heating. Sintering experiments carried out on alumina powder, both with and without applied pressure, revealed that the pressure-assisted process significantly improved densification, yielding near-complete density and increased hardness (21.6 GPa), while maintaining fine microstructures. This method highlights the potential of microwave-assisted sinter-forging for producing advanced ceramics with improved properties.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
Journal of The European Ceramic Society
Journal of The European Ceramic Society 工程技术-材料科学:硅酸盐
CiteScore
10.70
自引率
12.30%
发文量
863
审稿时长
35 days
期刊介绍: The Journal of the European Ceramic Society publishes the results of original research and reviews relating to ceramic materials. Papers of either an experimental or theoretical character will be welcomed on a fully international basis. The emphasis is on novel generic science concerning the relationships between processing, microstructure and properties of polycrystalline ceramics consolidated at high temperature. Papers may relate to any of the conventional categories of ceramic: structural, functional, traditional or composite. The central objective is to sustain a high standard of research quality by means of appropriate reviewing procedures.
期刊最新文献
An effective strategy for improving temperature stability of millimeter-wave dielectric ceramics realized in cordierite-rutile composites Ultra-high dynamic strength of submicron diamond-SiC composite Ultra-low temperature fabrication of Si3N4 porous structure with interconnected open mesopores through an alkali-activation-assisted crosslinking of native silica Microstructural insights into the CMAS corrosion resistance of ytterbium aluminum garnet doped with ytterbium oxide Structural insights and proton transport features in a hexagonal Ba5Ho2Al2SnO13 perovskite
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1