热变形参数对TAS31608/LH奥氏体不锈钢动态再结晶机理的影响

IF 3.9 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Journal of Materials Science Pub Date : 2025-02-18 DOI:10.1007/s10853-024-10336-w
Pengbo Hui, Guizhi Xiao, Haodong Chen, Chan He, Libo Tong, Zheng Zhang, Dening Zou
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引用次数: 0

摘要

液氢储罐用板应用于超低温和恶劣腐蚀环境,要求其微观结构均匀。高温轧制直接影响连铸坯的组织演变。通过热压缩试验,研究了TAS31608/LH奥氏体不锈钢在1000 ~ 1200℃、应变速率0.01 ~ 10 s−1范围内的热变形行为。利用Gleeble热机械模拟器进行了热压缩试验,并用电子背散射衍射(EBSD)对其微观结构进行了表征。研究了温度和应变速率对动态再结晶(DRX)机理的影响。结果表明,连续动态再结晶(CDRX)是热变形过程中的辅助再结晶机制,不连续动态再结晶(DDRX)是主要的再结晶机制。随着温度和应变速率的升高,低角晶界(LAGB)向高角晶界(HAGB)转变,孪晶和DRX的比例逐渐增加。此外,残余的δ-铁氧体促进了DDRX行为。δ-铁素体阻碍了再结晶晶粒的生长,导致混合晶体的出现。由于DRX在高温和应变速率下的促进作用,1200°C-10 s−1是TAS31608/LH的最佳热变形参数。
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Effect of hot deformation parameters on the dynamic recrystallization mechanism of TAS31608/LH austenitic stainless steels

Plates for liquid hydrogen storage tanks are used in ultra-low temperature and harsh corrosive environments, which require uniform microstructure. The microstructure evolution of continuous casting billets is directly impacted by high-temperature rolling. Herein, the hot deformation behavior of TAS31608/LH austenitic stainless steel is studied by hot compression tests in the temperature range of 1000–1200 °C and the strain rate range of 0.01 − 10 s−1. The hot compression test is carried out by the Gleeble thermal mechanical simulator, and the microstructure is characterized by electron backscatter diffraction (EBSD). The effect of the temperature and strain rate on the dynamic recrystallization (DRX) mechanism is demonstrated. The results suggest that the continuous dynamic recrystallization (CDRX) is the auxiliary DRX mechanism, and the discontinuous dynamic recrystallization (DDRX) is the principal DRX mechanism during hot deformation. When the temperature and strain rate increase, the low-angle grain boundary (LAGB) shifts to the high-angle grain boundary (HAGB), and the proportion of twins and DRX gradually increased. Additionally, residual δ-ferrite promotes the DDRX behavior. However, δ-ferrite hinder the growth of recrystallized grains, which lead to the appearance of the mixed crystals. Due to the promotion under high temperatures and strain rates for DRX, the 1200 °C–10 s−1 is the optimal hot deformation parameter of the TAS31608/LH.

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来源期刊
Journal of Materials Science
Journal of Materials Science 工程技术-材料科学:综合
CiteScore
7.90
自引率
4.40%
发文量
1297
审稿时长
2.4 months
期刊介绍: The Journal of Materials Science publishes reviews, full-length papers, and short Communications recording original research results on, or techniques for studying the relationship between structure, properties, and uses of materials. The subjects are seen from international and interdisciplinary perspectives covering areas including metals, ceramics, glasses, polymers, electrical materials, composite materials, fibers, nanostructured materials, nanocomposites, and biological and biomedical materials. The Journal of Materials Science is now firmly established as the leading source of primary communication for scientists investigating the structure and properties of all engineering materials.
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