水热合成Bi2S3-C点纳米复合材料的光催化性能增强

IF 3.4 4区 化学 Q3 CHEMISTRY, PHYSICAL Ionics Pub Date : 2025-01-31 DOI:10.1007/s11581-025-06105-7
Babita Tripathi, Sunil Chauhan, M. Z. A. Yahya, S. N. F. Yusuf, Markus Diantoro, R. C. Singh
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引用次数: 0

摘要

本文采用低温水热法制备了Bi2S3-xC点(x = 0、0.03、0.06、0.13、0.27、0.67和1.0)纳米复合材料样品。XRD测量证实了合成样品的相纯度和纳米复合性质。FESEM和TEM测试证实,原始Bi2S3和非晶C点同种异体接枝Bi2S3- xc点样品具有棒状形态,其尺寸(直径)在15 ~ 30 nm之间。研究了Bi2S3-xC纳米复合材料对环丙沙星(CIP)抗生素的光催化性能。x = 0.67的样品显示出最大的光催化活性(最大88%的CIP降解,在80分钟内),由于有效的电子转移和减少了纳米复合材料之间形成的p-n结的电荷重组率。
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Enhanced photocatalytic properties of hydrothermally synthesized Bi2S3-C dots nanocomposites

In this present communication, we have synthesized the Bi2S3-xC dots (x = 0, 0.03, 0.06, 0.13, 0.27, 0.67 and 1.0) nanocomposite samples by using low temperature hydrothermal method. The XRD measurements confirmed the phase purity and nanocomposite nature of the synthesized samples. FESEM and TEM measurements confirmed that, Bi2S3 samples have rod shape of morphology and their sizes (diameter) are between 15-30 nm in pristine Bi2S3 and Bi2S3-xC dots samples allografted with amorphous C dots. The photocatalytic properties of the Bi2S3-xC dots nanocomposite samples against the ciprofloxacin (CIP) antibiotic were studied in detail. The maximum photocatalytic activity was shown by x = 0.67 sample (maximum 88% CIP degradation, in 80 min) due to effective electrons transfer and reduction of charge recombination rate in the p–n junction, formed between the nanocomposite.

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来源期刊
Ionics
Ionics 化学-电化学
CiteScore
5.30
自引率
7.10%
发文量
427
审稿时长
2.2 months
期刊介绍: Ionics is publishing original results in the fields of science and technology of ionic motion. This includes theoretical, experimental and practical work on electrolytes, electrode, ionic/electronic interfaces, ionic transport aspects of corrosion, galvanic cells, e.g. for thermodynamic and kinetic studies, batteries, fuel cells, sensors and electrochromics. Fast solid ionic conductors are presently providing new opportunities in view of several advantages, in addition to conventional liquid electrolytes.
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