一种生产干燥颗粒表面均匀沉积的自动化系统。

J T Antley, R W Vanderpool, S L Harper
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引用次数: 1

摘要

一个实验室系统已经建成,均匀沉积干燥颗粒到任何类型的测试表面。作为一种质量保证工具,用于评估铅的表面采样方法,它也可用于为任何使用颗粒或灰尘作为运输机制的污染物生成测试表面。此外,它还可用于刺穿表面,用于有关粒子传输、再悬浮、再夹带和暴露的研究。机电系统包括一个坚固的铝室外壳沉积设备,一个计算机控制的定位系统,和一个0.61 x 0.61米的目标表面积(2 x 2英尺)。用于评估系统的介质包括各种尺寸的玻璃珠(物理直径在30到500微米之间)和亚利桑那测试粉尘(空气动力学直径在1到80微米之间)。预先的粒度分数可以单独用于研究单分散颗粒的影响,也可以混合使用以创建定制的多分散粒度分布。利用放置在表面的16个薄片阵列,从每次测试中收集有代表性的样品,可以量化颗粒沉积的均匀性。对于上述16种颗粒类型和大小以及各种总表面负荷(0.3-19 g/m2),该系统的平均变异系数小于20%。系统的可重复性计算(即在多个相同配置的运行中比较单个接合面位置的质量增益的平均变异系数)产生了大约10 +/- 5%(一个标准差)。系统的准确度测试,定义为预测表面载荷与实际载荷之间的绝对百分比差,结果为3.7±1.3%(一个标准差)。
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An automated system for producing uniform surface deposits of dry particles.

A laboratory system has been constructed that uniformly deposits dry particles onto any type of test surface. Devised as a quality assurance tool for the purpose of evaluating surface sampling methods for lead, it also may be used to generate test surfaces for any contaminant that uses particles or dust as a transport mechanism. Additionally, it may be used to spike surfaces for studies concerning particle transport, resuspension, reentrainment, and exposure. The electromechanical system includes a rugged aluminum chamber housing deposition equipment, a computer-controlled positioning system, and a 0.61 x 0.61 m target surface area (2 x 2 ft). Media used to evaluate the system have included glass beads of various size fractions (physical diameters between 30 and 500 microm), and Arizona Test Dust (aerodynamic diameters between 1 and 80 microm). Presieved particle size fractions may be used individually to study the effects of monodisperse particles, or may be mixed to create custom polydisperse size distributions. Using arrays of 16 coupons placed on the surface to collect representative samples from every test, the uniformity of the particle deposition can be quantified. The system achieved an average coefficient of variation of less than 20% for the 16 coupons for the particle types and sizes mentioned above and for a variety of total surface loadings (0.3-19 g/m2). Calculations of the system's repeatability (as the average coefficient of variation of mass gains for individual coupon locations compared across multiple identically configured runs) yielded approximately 10 +/- 5% (one standard deviation). Tests of the system's accuracy, defined as the absolute percentage difference between predicted surface loadings and actual loadings, yielded 3.7 +/- 1.3% (one standard deviation).

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