食品模拟溶液、涂刷和染色对复合树脂颜色稳定性的综合影响。

Acta Biomaterialia Odontologica Scandinavica Pub Date : 2017-01-16 eCollection Date: 2017-01-01 DOI:10.1080/23337931.2016.1276838
Tânia Mara Da Silva, Ana Luísa Leme Simões Sales, Cesar Rogerio Pucci, Alessandra Bühler Borges, Carlos Rocha Gomes Torres
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引用次数: 37

摘要

目的:研究食物模拟介质对不同复合树脂颜色稳定性的影响。材料和方法:每种复合材料制备80个样品:Grandio SO (Voco), Amaris (Voco), Filtek Z350XT (3M/ESPE), Filtek P90 (3M/ESPE)。按模拟食物介质分为4组,分别为人工唾液(对照)、庚烷、柠檬酸和乙醇。复合材料表面在自动牙刷机上进行10950次(200g负荷)的刷牙。用咖啡溶液在37°C下使样品变暗24 h。每次处理后,采用CIE L*a*b*系统分光光度法测定颜色。在基线(C1)和处理(食物模拟介质浸泡/C2,涂刷/C3和染料溶液/C4)后,测定每个标本的总体颜色变化(ΔE)。数据分析采用双向重复测量方差分析和Tukey检验(p < 0.05)。结果:RM-ANOVA分析结果显示,复合材料(p = .001)、时间(p = .001)和化学降解(p = .002)具有显著差异。复合材料ΔE的平均值为:Z350XT (5.39)a, Amaris (3.89)b, Grandio (3.75)bc, P90 (3.36)c。根据食物模拟介质:庚烷(4.41)a,柠檬酸(4.24)a,乙醇(4.02)ab,人工唾液(3.76)b。处理方法:染料溶液(4.53)a,涂刷(4.26)a,食物模拟培养基(3.52)b。结论:Filtek Z350XT复合树脂的染色效果明显高于其他复合树脂。浸泡在庚烷和柠檬酸中产生的颜色变化比其他食物模拟介质最大。样品暴露于涂刷方案和在咖啡溶液中变暗导致复合树脂的显着颜色变化。
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The combined effect of food-simulating solutions, brushing and staining on color stability of composite resins.

Objective: This study evaluated the effect of food-simulating media associated with brushing and coffee staining on color stability of different composite resins. Materials and methods: Eighty specimens were prepared for each composite: Grandio SO (Voco), Amaris (Voco), Filtek Z350XT (3M/ESPE), Filtek P90 (3M/ESPE). They were divided into four groups according to food-simulating media for 7 days: artificial saliva (control), heptane, citric acid and ethanol. The composite surface was submitted to 10,950 brushing cycles (200 g load) in an automatic toothbrushing machine. The specimens were darkened with coffee solution at 37 °C for 24 h. After each treatment, color measurements were assessed by spectrophotometry, using CIE L*a*b* system. The overall color change (ΔE) was determined for each specimen at baseline (C1) and after the treatments (food-simulating media immersion/C2, brushing/C3 and dye solution/C4). Data were analyzed by two-way repeated measures ANOVA and Tukey's tests (p < .05). Results: The results of RM-ANOVA showed significant differences for composites (p = .001), time (p = .001) and chemical degradation (p = .002). The mean of ΔE for composites were: Z350XT (5.39)a, Amaris (3.89)b, Grandio (3.75)bc, P90 (3.36)c. According to food-simulating media: heptane (4.41)a, citric acid (4.24)a, ethanol (4.02)ab, artificial saliva (3.76)b. For the treatments: dye solution (4.53)a, brushing (4.26)a, after food-simulating media (3.52)b. Conclusions: The composite resin Filtek Z350XT showed significantly higher staining than all other composite resin tested. The immersion in heptane and citric acid produced the highest color alteration than other food-simulating media. The exposure of samples to brushing protocols and darkening in coffee solution resulted in significant color alteration of the composite resins.

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