光固化切碎纤维增强牙科复合材料的力学测试。

Richard C Petersen, Edward G Wenski
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摘要

目的是验证将切碎的纤维加入到商用微粒填充的可见光固化牙膏中对强度的改善效果。在两种通用商用复合材料(3M 公司的 Z100 和 Kerr 公司的 Z100)中混合了光固化树脂预浸渍的 3 毫米高纯度石英纤维。Z100 和 Kerr Corp.XRV 的纤维含量为 35 wt%。在 2×2×25 毫米的模具中制备了四组试样,包括 Z100 和 XRV 对照组,以及含有纤维的 Z100 和 XRV 组,然后在 Demetron 辐射计监测的等效辐照强度下固化。根据 ASTM 标准 C 1161-94 配置-A,利用全关节四点弯曲夹具和 20 毫米跨度,对四个不同类别的十个试样进行了评估。根据 ASTM D 256-00 标准,使用改进型伊佐德塑料冲击试验机对每组中的五个样品进行了进一步评估。在最大弯曲应力、弯曲模量、断裂功和伊佐德冲击韧性方面,两种高度强化的纤维增强复合材料与商用对照组相比,都达到了统计学意义上的不确定边际误差(P=0.001 AVOVA posthoc Newman-Keuls)。从这些结果中可以得出结论,光固化切碎纤维增强复合材料与颗粒填充复合材料相比将产生突破性的改进。
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MECHANICAL TESTING OF A PHOTOCURED CHOPPED FIBER REINFORCED DENTAL COMPOSITE.

The objective was to validate strength improvements by incorporating chopped fiber into commercial particulate filled visible-light cured dental pastes. Photocurable resin preimpregnated 3-mm high purity quartz fibers were blended into two universal commercial composites, 3M Corp. Z100 and Kerr Corp. XRV at 35 wt% fiber. Four groups, consisting of the Z100 and XRV controls, along with Z100 and XRV both containing fibers, were prepared in a mold 2×2×25-mm then cured at equivalent irradiation intensities monitored by a Demetron Radiometer. Evaluation was accomplished on ten specimens from the four different categories according to ASTM Standard C 1161-94 configuration-A utilizing a fully-articulated four-point bend fixture and 20-mm span. Five samples out of each group were further assessed using a modified Izod Plastic Impact Tester per ASTM D 256-00. Both highly strengthened fiber reinforced composites attained a marginal error of uncertainty for statistical significance over the commercial controls (p=0.001 AVOVA posthoc Newman-Keuls) with maximum bending stress, flexural modulus, work of fracture and Izod impact toughness. From the results, it can be concluded that photocured chopped fiber reinforced composites will produce improvements over particulate filled compounds that can be considered breakthrough.

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MECHANICAL TESTING OF A PHOTOCURED CHOPPED FIBER REINFORCED DENTAL COMPOSITE.
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