遮光固化方式对硅烷基与甲基丙烯酸酯基树脂复合材料转化率的影响。

Journal of Dental Biomaterial Pub Date : 2016-12-01
Mousavinasab Sm, Atai M, Salehi N, Salehi A
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引用次数: 0

摘要

问题陈述:转换程度取决于材料成分、光源特性、与光源的距离、光强、固化时间以及阴影和半透明等其他因素。目的:在本研究中,我们评估了不同的光固化模式和阴影的甲基丙烯酸酯和硅烷基树脂复合材料对树脂复合材料的转化率(DC)的影响。材料和方法:采用甲基丙烯酸酯基(Filtek Z250、3M、ESPE)和低收缩率硅烷基(Filtek P90、3M、ESPE)树脂复合材料,分为3组:1-Filtek Z250组(阴影A3)、2-Filtek Z250组(阴影B2)和3-Filtek P90组(阴影A3)。我们使用发光二极管(LED)固化单元进行光聚合。每组取10个样品,评价转化程度;5个样品采用软启动固化方式固化,另外5个样品采用标准固化方式固化。利用傅里叶变换红外光谱(FTIR)测定了树脂复合材料的直流电(DC)。数据分析采用Kruskal Wallis和单因素方差分析统计检验。结果:硅烷基树脂复合材料转化率为70 ~ 75.8%,甲基丙烯酸酯基树脂复合材料转化率为60.2 ~ 68.2% (p = 0.009)。颜色较亮的复合材料(B2)的转换程度在统计学上大于颜色较暗的复合材料(A3)。采用标准固化方式可获得较高的转化率。结论:研究结果表明,树脂复合材料的颜色、种类以及固化方式影响树脂复合材料的转化程度。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

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Effect of Shade and Light Curing Mode on the Degree of Conversion of Silorane-Based and Methacrylate-Based Resin Composites.

Statement of problem: The degree of conversion depends on the material composition, light source properties, distance from light source, light intensity, curing time, and other factors such as shade and translucency.

Objectives: In the present study, we evaluated the effects of different light-curing modes and shades of methacrylate and silorane-based resin composites on the degree of conversion of resin composites (DC).

Materials and methods: The methacrylate-based (Filtek Z250, 3M, ESPE) and low-shrinkage silorane-based (Filtek P90, 3M, ESPE) resin composites were used in three groups as follows: group 1-Filtek Z250 (shade A3), group 2-Filtek Z250 (shade B2), and group 3-Filtek P90 (shade A3). We used a light-emitting diode (LED) curing unit for photopolymerization. 10 samples were prepared in each group to evaluate the degree of conversion; 5 samples were cured using soft-start curing mode, and the other 5 were cured using standard curing mode. The DC of the resin composites was measured using Fourier Transform Infrared Spectroscopy (FTIR). The data were analyzed using Kruskal Wallis and one-way ANOVA statistical tests.

Results: The degree of conversion of silorane-based resin composite was 70 - 75.8% and that of methacrylate-based resin composites was 60.2 - 68.2% (p = 0.009). The degree of conversion of the composite with brighter colour (B2) was statistically more than the darker composite (A3). Higher degree of conversion was achieved applying the standard curing mode.

Conclusions: The results of the study showed that the colour and type of the resin composite and also the curing mode influence the degree of conversion of resin composites.

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