John P Sutter, Philip A Chater, Riccardo Signorato, Dean S Keeble, Michael R Hillman, Matthew G Tucker, Simon G Alcock, Ioana-Theodora Nistea, Heribert Wilhelm
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引用次数: 7
摘要
金刚石光源(DLS)光束线I15-1利用40-80 keV x射线的散射测量原子对分布函数(PDF)。在样品和检测器之间的可变位置,需要一种独特的聚焦元件将这些x射线从最初的大截面(11.0 mm H × 4.2 mm V)凝聚成所需的光斑尺寸FWHM≈680 μm (H) × 20 μm (V)。大数值孔径是通过在超过1 m长的硅衬底上涂覆三层布拉格角为4.2 mrad的多层条纹来实现的。一条条纹选择能量分别为40.0、65.4和76.6 keV的x射线。16个压电双晶片驱动器附着在镜子衬底的两侧,调整反射表面的形状。在0.92 m范围内的三个位置获得垂直宽度< 15µm的焦点,可以快速,轻松地从一个焦点位置切换到另一个焦点位置。在减去均匀曲率后,最小均方根斜率误差接近0.5µrad。反射率曲线沿各条纹呈现一致的峰值,峰值位置的角度变化较小。这是在同步加速器光束线上首次应用1米长的多层涂层双晶片反射镜。在它的帮助下,在锂离子电池阴极的切片上收集了数据。
1 m long multilayer-coated deformable piezoelectric bimorph mirror for adjustable focusing of high-energy X-rays.
The Diamond Light Source (DLS) beamline I15-1 measures atomic pair distribution functions (PDF) using scattering of 40-80 keV X-rays. A unique focusing element was needed to condense these X-rays from an initial large cross section (11.0 mm H × 4.2 mm V) into a required spot size of FWHM ≈680 μm (H) × 20 μm (V) at a variable position between the sample and the detector. The large numerical aperture is achieved by coating a silicon substrate over 1 m long with three multilayer stripes of Bragg angle 4.2 mrad. One stripe selects X-rays of each energy 40.0, 65.4, and 76.6 keV. Sixteen piezoelectric bimorph actuators attached to the sides of the mirror substrate adjusted the reflecting surface's shape. Focal spots of vertical width < 15 µm were obtained at three positions over a 0.92 m range, with fast, easy switching from one focal position to another. Minimized root mean square slope errors were close to 0.5 µrad after subtraction of a uniform curvature. Reflectivity curves taken along each stripe showed consistent high peaks with generally small angular variation of peak positions. This is the first application of a 1 m long multilayer-coated bimorph mirror at a synchrotron beamline. Data collected with its help on a slice of a lithium ion battery's cathode are presented.
期刊介绍:
Optics Express is the all-electronic, open access journal for optics providing rapid publication for peer-reviewed articles that emphasize scientific and technology innovations in all aspects of optics and photonics.