{"title":"硝酸铋诱导微波辅助姜黄素快速合成香兰素。","authors":"Debasish Bandyopadhyay, Bimal K Banik","doi":"10.1186/2191-2858-2-15","DOIUrl":null,"url":null,"abstract":"<p><strong>Background: </strong>Curcumin and vanillin are the two useful compounds in food and medicine. Bismuth nitrate pentahydrate is an economical and ecofriendly reagent.</p><p><strong>Method: </strong>Bismuth nitrate pentahydrate impregnated montmorillonite KSF clay and curcumin were subjected to microwave irradiation.</p><p><strong>Results: </strong>Microwave-induced bismuth nitrate-promoted synthesis of vanillin from curcumin has been accomplished in good yield under solvent-free condition. Twenty-five different reaction conditions have been studied to optimize the process.</p><p><strong>Conclusion: </strong>The present procedure for the synthesis of vanillin may find useful application in the area of industrial process development.</p>","PeriodicalId":19639,"journal":{"name":"Organic and Medicinal Chemistry Letters","volume":" ","pages":"15"},"PeriodicalIF":0.0000,"publicationDate":"2012-04-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1186/2191-2858-2-15","citationCount":"12","resultStr":"{\"title\":\"Bismuth nitrate-induced microwave-assisted expeditious synthesis of vanillin from curcumin.\",\"authors\":\"Debasish Bandyopadhyay, Bimal K Banik\",\"doi\":\"10.1186/2191-2858-2-15\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><strong>Background: </strong>Curcumin and vanillin are the two useful compounds in food and medicine. Bismuth nitrate pentahydrate is an economical and ecofriendly reagent.</p><p><strong>Method: </strong>Bismuth nitrate pentahydrate impregnated montmorillonite KSF clay and curcumin were subjected to microwave irradiation.</p><p><strong>Results: </strong>Microwave-induced bismuth nitrate-promoted synthesis of vanillin from curcumin has been accomplished in good yield under solvent-free condition. Twenty-five different reaction conditions have been studied to optimize the process.</p><p><strong>Conclusion: </strong>The present procedure for the synthesis of vanillin may find useful application in the area of industrial process development.</p>\",\"PeriodicalId\":19639,\"journal\":{\"name\":\"Organic and Medicinal Chemistry Letters\",\"volume\":\" \",\"pages\":\"15\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2012-04-20\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1186/2191-2858-2-15\",\"citationCount\":\"12\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Organic and Medicinal Chemistry Letters\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1186/2191-2858-2-15\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Organic and Medicinal Chemistry Letters","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1186/2191-2858-2-15","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Bismuth nitrate-induced microwave-assisted expeditious synthesis of vanillin from curcumin.
Background: Curcumin and vanillin are the two useful compounds in food and medicine. Bismuth nitrate pentahydrate is an economical and ecofriendly reagent.
Method: Bismuth nitrate pentahydrate impregnated montmorillonite KSF clay and curcumin were subjected to microwave irradiation.
Results: Microwave-induced bismuth nitrate-promoted synthesis of vanillin from curcumin has been accomplished in good yield under solvent-free condition. Twenty-five different reaction conditions have been studied to optimize the process.
Conclusion: The present procedure for the synthesis of vanillin may find useful application in the area of industrial process development.
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