改良丝网印刷电极测定维生素C:在实际样品中检测维生素C的应用

IF 1.1 Q4 ELECTROCHEMISTRY Surface Engineering and Applied Electrochemistry Pub Date : 2021-09-01 DOI:10.3103/S1068375521040141
Fatemeh Shayanfar,  Hamid Sarhadi
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引用次数: 2

摘要

在本研究中,使用磁性纳米ZnFe2O4修饰丝网印刷电极。改性电极降低了维生素C的过电位(70 mV),显著提高了其氧化峰电流(3.3%)。在最佳条件下,采用差分脉冲伏安法,电极在维生素C浓度0.5 ~ 500.0 μM范围内呈线性响应,检出限为0.15 µM。该电极具有良好的线性范围和微摩尔检测限,灵敏度高,稳定性和重复性好等优良的电化学性能。通过对实际样品中维生素C浓度的定量分析,揭示了该方法的实用性。
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Determination of Vitamin C at Modified Screen Printed Electrode: Application for Sensing of Vitamin C in Real Samples

In this study, ZnFe2O4 magnetic nanoparticles were used to modify a screen printed electrode. The modified electrode decreased the over-potential of vitamin C (70 mV) and prominently increased its oxidation peak current (3.3%). Under optimum conditions, the electrode provided a linear response based on the vitamin C concentrations between 0.5–500.0 μM, with a detection limit of 0.15 µM, by using the differential pulse voltammetric method. The modified electrode exhibited excellent electrochemical performance, including a good linear range and a micromolar detection limit, high sensitivity, and desirable stability and repeatability. Particularly, the practical applicability was revealed by quantifying the vitamin C concentrations in real samples.

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来源期刊
Surface Engineering and Applied Electrochemistry
Surface Engineering and Applied Electrochemistry Engineering-Industrial and Manufacturing Engineering
CiteScore
1.70
自引率
22.20%
发文量
54
审稿时长
6 months
期刊介绍: Surface Engineering and Applied Electrochemistry is a journal that publishes original and review articles on theory and applications of electroerosion and electrochemical methods for the treatment of materials; physical and chemical methods for the preparation of macro-, micro-, and nanomaterials and their properties; electrical processes in engineering, chemistry, and methods for the processing of biological products and food; and application electromagnetic fields in biological systems.
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