Renata Vasconcelos Monteiro, Daniela Micheline Dos Santos, Bruna Chrispim, Jussara Karina Bernardon, Thiago Soares Porto, Grace Mendonça De Souza
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The bonded specimens were stored in water for 24 h, 6 months, or 1 year and subjected to microshear bond strength testing. The data were analyzed by one-way ANOVA and Tukey's test (p < 0.05). The contact angle was measured after adhesive application to evaluate surface wettability. The adhesive-treated specimens were analyzed with x-ray photoelectron spectroscopy (XPS) and time-of-flight secondary ion mass spectrometry (ToF-SIMS) for chemical characterization.</p><p><strong>Results: </strong>The application of a 10-MDP-based adhesive significantly improved bond strength of composite cement to zirconia when compared to the control group (no adhesive application) (p < 0.05). One-year water storage significantly decreased bond strength for ABU- and CUB-bonded specimens, but not for SUA-bonded specimens. The analysis by XPS and ToF-SIMS showed peaks of carbon, phosphorus, and silicon in all adhesive-treated specimens.</p><p><strong>Conclusions: </strong>One-year water storage affected the bond strength of composite cement to zirconia when All Bond Universal or Clearfil Universal Bond Quick were used.</p>","PeriodicalId":2,"journal":{"name":"ACS Applied Bio Materials","volume":" ","pages":"385-394"},"PeriodicalIF":4.7000,"publicationDate":"2022-10-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11734258/pdf/","citationCount":"0","resultStr":"{\"title\":\"Effect of Universal Adhesives on Long-term Bond Strength to Zirconia.\",\"authors\":\"Renata Vasconcelos Monteiro, Daniela Micheline Dos Santos, Bruna Chrispim, Jussara Karina Bernardon, Thiago Soares Porto, Grace Mendonça De Souza\",\"doi\":\"10.3290/j.jad.b3512333\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><strong>Purpose: </strong>To evaluate the effect of universal adhesives on the long-term bond strength to yttria-stabilized tetragonal zirconia polycrystal (Y-TZP).</p><p><strong>Materials and methods: </strong>Polyethylene tubes filled with composite cement containing 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP) were adhesively luted to 60 fully sintered Y-TZP slabs (7 x 7 x 2 mm) with or without (control) previous application of a 10-MDP-based adhesive (All Bond Universal, Bisco) - ABU; Clearfil Universal Bond Quick, Kuraray Noritake - CUB; Scotchbond Universal Adhesive, 3M Oral Care - SUA) on the zirconia surface. 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引用次数: 0
摘要
目的：评估通用粘合剂对钇稳定四方氧化锆多晶体（Y-TZP）长期粘合强度的影响：将装有含 10-甲基丙烯酰氧癸基磷酸二氢酯（10-MDP）的复合粘合剂的聚乙烯管与 60 块完全烧结的 Y-TZP 板（7 x 7 x 2 毫米）粘接在一起，并在氧化锆表面涂抹或不涂抹（对照组）以 10-MDP 为基础的粘合剂（All Bond Universal，Bisco）- ABU；Clearfil Universal Bond Quick，Kuraray Noritake - CUB；Scotchbond Universal Adhesive，3M Oral Care - SUA）。粘结后的试样在水中分别存放 24 小时、6 个月或 1 年，然后进行微剪切粘结强度测试。数据分析采用单因素方差分析和 Tukey 检验（P < 0.05）。使用粘合剂后测量接触角以评估表面润湿性。用 X 射线光电子能谱（XPS）和飞行时间二次离子质谱（ToF-SIMS）分析粘合剂处理过的试样的化学特性：与对照组（未使用粘合剂）相比，使用基于 10-MDP 的粘合剂可显著提高复合水泥与氧化锆的粘结强度（p < 0.05）。ABU和CUB粘结试样一年的水贮存会明显降低粘结强度，而SUA粘结试样则不会。XPS 和 ToF-SIMS 分析显示，在所有粘合剂处理过的试样中都出现了碳、磷和硅的峰值：结论：使用 All Bond Universal 或 Clearfil Universal Bond Quick 时，一年的储水会影响复合水泥与氧化锆的粘接强度。
Effect of Universal Adhesives on Long-term Bond Strength to Zirconia.
Purpose: To evaluate the effect of universal adhesives on the long-term bond strength to yttria-stabilized tetragonal zirconia polycrystal (Y-TZP).
Materials and methods: Polyethylene tubes filled with composite cement containing 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP) were adhesively luted to 60 fully sintered Y-TZP slabs (7 x 7 x 2 mm) with or without (control) previous application of a 10-MDP-based adhesive (All Bond Universal, Bisco) - ABU; Clearfil Universal Bond Quick, Kuraray Noritake - CUB; Scotchbond Universal Adhesive, 3M Oral Care - SUA) on the zirconia surface. The bonded specimens were stored in water for 24 h, 6 months, or 1 year and subjected to microshear bond strength testing. The data were analyzed by one-way ANOVA and Tukey's test (p < 0.05). The contact angle was measured after adhesive application to evaluate surface wettability. The adhesive-treated specimens were analyzed with x-ray photoelectron spectroscopy (XPS) and time-of-flight secondary ion mass spectrometry (ToF-SIMS) for chemical characterization.
Results: The application of a 10-MDP-based adhesive significantly improved bond strength of composite cement to zirconia when compared to the control group (no adhesive application) (p < 0.05). One-year water storage significantly decreased bond strength for ABU- and CUB-bonded specimens, but not for SUA-bonded specimens. The analysis by XPS and ToF-SIMS showed peaks of carbon, phosphorus, and silicon in all adhesive-treated specimens.
Conclusions: One-year water storage affected the bond strength of composite cement to zirconia when All Bond Universal or Clearfil Universal Bond Quick were used.
期刊介绍：
ACS Applied Bio Materials is an interdisciplinary journal publishing original research covering all aspects of biomaterials and biointerfaces including and beyond the traditional biosensing, biomedical and therapeutic applications.
The journal is devoted to reports of new and original experimental and theoretical research of an applied nature that integrates knowledge in the areas of materials, engineering, physics, bioscience, and chemistry into important bio applications. The journal is specifically interested in work that addresses the relationship between structure and function and assesses the stability and degradation of materials under relevant environmental and biological conditions.
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