Rahisa Mohammed, Peace Ogadi, Dennis M Seth, Amrutaa Vibho, Sarah K Gallant, Rory Waterman
{"title":"2-（（（2,7-二羟基萘-1-基）亚甲基）氨基-3'，6'-双（乙基氨基）-2'，7'-二甲基螺[异吲哚啉-1,9'-黄嘌呤]-3-酮的合成、表征及水中铀的比色检测。","authors":"Rahisa Mohammed, Peace Ogadi, Dennis M Seth, Amrutaa Vibho, Sarah K Gallant, Rory Waterman","doi":"10.3390/m1725","DOIUrl":null,"url":null,"abstract":"<p><p>2-(((2,7-Dihydroxynaphthalen-1-yl)methylene)amino)-3',6'-bis(ethylamino)-2',7'-dimethyl-spiro[isoindoline-1,9'-xanthen]-3-one was synthesized using Rhodamine 6G hydrazide (prepared using literature methods) and commercially available 2,7-dihydroxynaphthalene-1-carbaldehyde via imine condensation. Structural characterization was performed using FT-IR, <sup>1</sup>H-NMR, <sup>13</sup>C-NMR, X-ray, and HRMS. This Schiff base shows promise as a ligand for the colorimetric analysis of uranium in water.</p>","PeriodicalId":18761,"journal":{"name":"Molbank","volume":"2023 3","pages":""},"PeriodicalIF":0.6000,"publicationDate":"2023-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10540563/pdf/","citationCount":"0","resultStr":"{\"title\":\"Synthesis and Characterization of 2-(((2,7-Dihydroxynaphthalen-1-yl)methylene)amino)-3',6'-bis(ethylamino)-2',7'-dimethylspiro[isoindoline-1,9'-xanthen]-3-one and Colorimetric Detection of Uranium in Water.\",\"authors\":\"Rahisa Mohammed, Peace Ogadi, Dennis M Seth, Amrutaa Vibho, Sarah K Gallant, Rory Waterman\",\"doi\":\"10.3390/m1725\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><p>2-(((2,7-Dihydroxynaphthalen-1-yl)methylene)amino)-3',6'-bis(ethylamino)-2',7'-dimethyl-spiro[isoindoline-1,9'-xanthen]-3-one was synthesized using Rhodamine 6G hydrazide (prepared using literature methods) and commercially available 2,7-dihydroxynaphthalene-1-carbaldehyde via imine condensation. Structural characterization was performed using FT-IR, <sup>1</sup>H-NMR, <sup>13</sup>C-NMR, X-ray, and HRMS. This Schiff base shows promise as a ligand for the colorimetric analysis of uranium in water.</p>\",\"PeriodicalId\":18761,\"journal\":{\"name\":\"Molbank\",\"volume\":\"2023 3\",\"pages\":\"\"},\"PeriodicalIF\":0.6000,\"publicationDate\":\"2023-09-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10540563/pdf/\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Molbank\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.3390/m1725\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"2023/9/15 0:00:00\",\"PubModel\":\"Epub\",\"JCR\":\"Q4\",\"JCRName\":\"CHEMISTRY, ORGANIC\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Molbank","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.3390/m1725","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2023/9/15 0:00:00","PubModel":"Epub","JCR":"Q4","JCRName":"CHEMISTRY, ORGANIC","Score":null,"Total":0}
Synthesis and Characterization of 2-(((2,7-Dihydroxynaphthalen-1-yl)methylene)amino)-3',6'-bis(ethylamino)-2',7'-dimethylspiro[isoindoline-1,9'-xanthen]-3-one and Colorimetric Detection of Uranium in Water.
2-(((2,7-Dihydroxynaphthalen-1-yl)methylene)amino)-3',6'-bis(ethylamino)-2',7'-dimethyl-spiro[isoindoline-1,9'-xanthen]-3-one was synthesized using Rhodamine 6G hydrazide (prepared using literature methods) and commercially available 2,7-dihydroxynaphthalene-1-carbaldehyde via imine condensation. Structural characterization was performed using FT-IR, 1H-NMR, 13C-NMR, X-ray, and HRMS. This Schiff base shows promise as a ligand for the colorimetric analysis of uranium in water.
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