安山岩玄武岩烧结制备高密度陶瓷

IF 0.9 4区 材料科学 Q3 MATERIALS SCIENCE, CERAMICS Processing and Application of Ceramics Pub Date : 2021-08-25 DOI:10.21203/rs.3.rs-827727/v1
V. Pavkov, G. Bakić, Vesna Maksimovic, I. Cvijović-Alagić, Marija Prekajski Đorđević, D. Bučevac, B. Matović
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引用次数: 2

摘要

现代工业要求不仅包括使用具有良好机械性能的建筑材料,还包括通过环境友好和低成本加工程序获得的材料。玄武岩作为一种低成本的原材料,被认为是工业建筑零件生产的良好候选材料。在本研究中,来源于塞尔维亚“Donje Jarinje”矿床的安山岩玄武岩被认为是高密度陶瓷生产的潜在原料。高密度陶瓷的生产包括干磨、均匀化、冷等静压和空气烧结。为了确定最佳工艺参数,烧结在1040、1050、1060、1070和1080°C下进行,然后在1060°C的最佳烧结温度下,烧结持续时间从30到240分钟不等。起始材料和烧结材料的表征包括颗粒尺寸分布、密度、硬度和断裂韧性的估计,并辅以X射线衍射、光学显微镜、扫描电子显微镜和能量色散光谱分析。在1040至1080°C的研究温度范围内,加工过程中没有发生相变。研究结果表明,在空气中1060°C烧结60min的安山岩玄武岩,其相对密度达到99.5%,硬度和断裂韧性最高,分别为6.7GPa和2.2MPaÖm。所提出的研究结果证实,烧结安山岩玄武岩可以用作各种工业应用的高密度陶瓷材料,因为这种环保材料显示出令人满意的机械性能。
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High-Density Ceramics Obtained By Andesite Basalt Sintering
Modern industrial requirements include not only the usage of constructive materials with good mechanical properties but also materials obtained through environmentally friendly and low-cost processing procedures. Basalt, as a low-cost raw material, is regarded as a good candidate for industrial constructive parts production. In the present study, andesite basalt originated from the deposit site "Donje Jarinje", Serbia, was examined as a potential raw material for high-density ceramics production. The production of high-density ceramics included dry milling, homogenization, cold isostatic pressing, and sintering in the air. To determine the optimal processing parameters the sintering was conducted at 1040, 1050, 1060, 1070, and 1080 °C, and afterward the sintering duration was varied from 30 to 240 min at the optimal sintering temperature of 1060 °C. Characterization of the starting and sintered materials included the estimation of particle size distribution, density, hardness, and fracture toughness complemented with X-ray diffraction, light optical microscopy, scanning electron microscopy, and energy dispersive spectroscopy analysis. Phase transformations did not occur during processing in the investigated temperature range from 1040 to 1080 °C. The obtained research results showed that 99.5% of relative density and the highest hardness and fracture toughness values of 6.7 GPa and 2.2 MPaÖm, respectively, were achieved for the andesite basalt sintered at 1060 °C for 60 min in the air. The results of the presented study confirmed that the sintered andesite basalt can be used as a high-density ceramic material for various industrial applications since this environmentally friendly material shows satisfactory mechanical properties.
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来源期刊
Processing and Application of Ceramics
Processing and Application of Ceramics MATERIALS SCIENCE, CERAMICS-
CiteScore
1.90
自引率
9.10%
发文量
14
审稿时长
10 weeks
期刊介绍: Information not localized
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