LDH- α - fe2o3 - mos2复合材料去除植物油和水中Pb2+的研究

F. Emen, R. E. Demirdöğen, G. Avsar, A. I. Karaçolak
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引用次数: 0

摘要

水污染是一个全球性的问题。无机和有机污染物是水资源中的主要污染物。因此,开发先进的吸附材料,有效地去除水中的金属和油,是人们非常关注的问题。本研究合成了一种新型LDH复合材料,用于吸附污染水体中的重金属和油类。为此,制备了MgAlOH- α - fe2o3 - mo_2复合材料,并通过FT-IR和XRD对其进行了表征。复合材料的XRD粉末谱图表明,复合材料中含有g - fe2o3 (PDF卡号:00-002-1047)、MgAl(OH)14。xh2o (PDF卡号:00-043-0072)和MoS 2 (PDF卡号:00-037-4492)。采用DTA/TG技术研究了复合材料的热稳定性。MgAlOH- α - fe2o3 - mo2o3复合材料对植物油的吸附效率可达其自重的418%。MgAlOH- α - fe2o3 - mo2o3复合材料去除水溶液中pb2 +离子的能力。ICP-OES测定pb2 +。考察了pb2 +用量、PH、吸附剂用量和溶剂流速对MgAlOH- α - fe2o3 - mo_2复合材料吸附性能的影响。
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LDH- ɣ-Fe2O3-MoS2 composite for Vegetable Oil and Pb2+ Removal From Water
Water pollution is a global concern. Inorganic and organic pollutants constitute primary pollutants in water resources. Therefore, it is of great concern to develop advanced sorbent materials for effective and efficient removal of metals and oil from water. In this study, synthesis of new LDH composites which would be used for sorption of heavy metals and oils from polluted water. For this purpose, MgAlOH- ɣ -Fe 2 O 3 -MoS 2 composite was prepared and characterized were made via FT-IR and XRD. The XRD powder pattern of the composite showed that it contained g -Fe 2 O 3 (PDF card no:00-002-1047), MgAl(OH)14.XH 2 O (PDF card no:00-043-0072) and MoS 2 (PDF card no:00-037-4492). Thermal stability of the composite was investigated via DTA/TG technique. MgAlOH- ɣ -Fe 2 O 3 -MoS 2 composite was shows highly efficient sorption for vegetable oil up to 418% times its own weight. The ablity of MgAlOH- ɣ -Fe 2 O 3 -MoS 2 composite for removing Pb 2+ ions from aqueous solution. Pb 2+ analysis was made by ICP-OES. The effect of Pb 2+ amounts, PH, sorbent amounts and solvent flow rate on t he adsorption capacity of MgAlOH- ɣ -Fe 2 O 3 -MoS 2 composite were also ivestigated.
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来源期刊
CiteScore
1.60
自引率
0.00%
发文量
81
审稿时长
5 weeks
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