磷掺杂ZnO纳米粒子的合成与表征

Pub Date : 2022-07-01 DOI:10.15251/jobm.2022.143.137
J. El Ghoul, N. Abdel All
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引用次数: 0

摘要

我们报道了通过溶胶-凝胶处理技术合成磷掺杂的ZnO纳米颗粒,磷浓度范围为2%至8%。通过不同的技术表征了这些纳米颗粒的结构和光学性质。结构研究证实了六方纤锌矿相的存在,平均晶粒尺寸约为30nm。然而,光学研究表明,在紫外线范围内具有高吸收率,在可见光范围内具有重要反射率。P-ZnO样品的光学带隙在3.32~3.28eV之间变化。本工作的目的是研究磷掺杂对ZnO纳米颗粒结构、形态和光学性能的影响。
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Synthesis and characterizations of phosphorus doped ZnO nanoparticles
We reported the synthesis of phosphorus doped ZnO nanoparticles for a concentration of P ranging from 2 to 8%by a sol–gel processing technique. The structural and optical properties of these nanoparticles were characterised by different techniques. The structural study confirms the presence of hexagonal wurtzite phase with average crystallite size around 30nm. However, the optical study was shown a high absorption in the UV range and an important reflectance in the visible range. The optical band gap of P-ZnO samples were varied between 3.32 and 3.28 eV. The aim of this work is to study the effect of phosphorus doping on the structural, morphological and optical properties of ZnO nanoparticles.
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