温度对不同类型有机硅粘度的影响

Q4 Medicine Journal of Plastination Pub Date : 2018-07-31 DOI:10.56507/hett9088
Y. F. Monteiro, L.S. Juvenato, V. ANAPAULAS., Bittencourt, Bruno Siqueira, F. C. Monteiro, C. A. Baptista, S. Athelson
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引用次数: 3

摘要

:本工作的目的是测试温度对塑化技术中常用的三种不同分子量的硅酮(Biodur®S10、Polsil®P10和P1)粘度的影响。在本研究中,使用RheolabQC模型旋转流变仪测量所选聚合物在以下温度下的动态粘度:-5、0、5、10、15、20、25、30和35°C。根据从每个样品获得的9次粘度测量,构建了粘度与温度的关系图。分析了每种聚合物的动态粘度曲线方程。与其他硅酮相比,Polsil®P1硅酮的粘度要低得多(25°C时约为80 mPa.s,-25°C时为550 mPa.s)。Polsil®P10有机硅在所分析的聚合物中表现出最高的粘度(在25°C时约为1180 mPa.s,在-25°C时为3730 mPa.s)。Biodur®的S10有机硅显示出中等粘度(25°C时约为410 mPa.s,-25°C时为1500 mPa.s)。我们得出的结论是,Polsil®P1有机硅具有高流动性和低粘度,因此在塑化测试中表现出了最佳的物理化学特性。值得注意的是,Polsil®P1在冷浸渍温度(-15°C)下的粘度仍低于Biodur®S10(对照)在室温(20-25°C)时的粘度。我们还得出结论,了解有机硅的内在和外在物理化学特性及其动态粘度,有助于选择用于低温或室温塑化技术的理想有机硅。
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Influence of the Temperature on the Viscosity of Different Types of Silicone
: The objective of this work was to test the influence of temperature on the viscosity of three silicones of different molecular weights (Biodur® S10, Polisil® P10 and P1) commonly used in the plastination technique. For the study, the RheolabQC model rotational rheometer was used to measure the dynamic viscosities of the chosen polymers at the following temperatures: -5, 0, 5, 10, 15, 20, 25, 30 and 35 °C. From the 9 measurements of viscosities obtained from each sample, a viscosity vs. temperature graph was constructed. The equation of the dynamic viscosity curve of each polymer was analyzed. Polisil® P1 silicone had a much lower viscosity compared to other silicones (about 80 mPa.s at 25 °C and 550 mPa.s at -25 °C). Polisil® P10 silicone presented the highest viscosity of the polymers analyzed (approximately 1180 mPa.s at 25 °C and 3730 mPa.s at -25 °C). The Biodur®'s S10 silicone showed an intermediate viscosity (about 410 mPa.s at 25 ° C and 1500 mPa.s at -25 °C). We conclude that Polisil® P1 silicone presented the best physico-chemical characteristics of the tested silicones for plastination, because it has high fluidity and low viscosity. It is noteworthy that the viscosity of Polisil® P1 in cold impregnation temperature (-15 °C) is still lower than the viscosity of the Biodur® S10 (control) at room temperature (20-25 °C). We also conclude that the knowledge of the intrinsic and extrinsic physicochemical characteristics of the silicone and its dynamic viscosity is helpful in choosing the ideal silicone for use in the cold or room temperature plastination techniques.
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来源期刊
Journal of Plastination
Journal of Plastination Health Professions-Medical Laboratory Technology
CiteScore
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