{"title":"通过验证的LC-MS/MS方法从牛至属植物Majorana（Mill.）Benth部分提取的酚类化合物","authors":"S. Carikci, A. Gören, T. Kilic, T. Dirmenci","doi":"10.25135/jcm.80.2211.2667","DOIUrl":null,"url":null,"abstract":"AbstrAbstract: Origanum majorana L., (OM), O. onites L. (OO) and O. syriacum L. (subsp. bevanii (Holmes) Greuter & Burdet) (OS) are belong to Majorana (Mill.) Benth. section of Origanum L. genus. In this study, quantities of some phenolic compounds; gallic acid, syringic acid, p -hydory benzoic acid, caffeic acid, ( E )-ferulic acid, chlorogenic acid, rosmarinic acid, pyrogallol and vanillin; in the chloroform (C), acetone (Ac) and methanol (M) extracts prepared from Origanum species collected from Türkiye were investigated via liquid chromatography and tandem mass spectrometry (LC-MS/MS). The relative standard deviations (RSD) of the phenolics were found as follows; 4.85, 8.39, 4.78, 8.04, 5.21, 5.45, 3.73, 5.47, respectively. Curcumin was used as an internal standard. In the extracts, ( E )-ferulic acid and caffeic acid were found to be the most abundant compounds. O. syriacum was determined as the richest species in terms of phenolic acids.","PeriodicalId":15343,"journal":{"name":"Journal of Chemical Metrology","volume":" ","pages":""},"PeriodicalIF":1.8000,"publicationDate":"2022-12-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Phenolic compounds from section Majorana (Mill.) Benth of Origanum L. species extracts via validated LC-MS/MS method\",\"authors\":\"S. Carikci, A. Gören, T. Kilic, T. Dirmenci\",\"doi\":\"10.25135/jcm.80.2211.2667\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"AbstrAbstract: Origanum majorana L., (OM), O. onites L. (OO) and O. syriacum L. (subsp. bevanii (Holmes) Greuter & Burdet) (OS) are belong to Majorana (Mill.) Benth. section of Origanum L. genus. In this study, quantities of some phenolic compounds; gallic acid, syringic acid, p -hydory benzoic acid, caffeic acid, ( E )-ferulic acid, chlorogenic acid, rosmarinic acid, pyrogallol and vanillin; in the chloroform (C), acetone (Ac) and methanol (M) extracts prepared from Origanum species collected from Türkiye were investigated via liquid chromatography and tandem mass spectrometry (LC-MS/MS). The relative standard deviations (RSD) of the phenolics were found as follows; 4.85, 8.39, 4.78, 8.04, 5.21, 5.45, 3.73, 5.47, respectively. Curcumin was used as an internal standard. In the extracts, ( E )-ferulic acid and caffeic acid were found to be the most abundant compounds. O. syriacum was determined as the richest species in terms of phenolic acids.\",\"PeriodicalId\":15343,\"journal\":{\"name\":\"Journal of Chemical Metrology\",\"volume\":\" \",\"pages\":\"\"},\"PeriodicalIF\":1.8000,\"publicationDate\":\"2022-12-31\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Chemical Metrology\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.25135/jcm.80.2211.2667\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"CHEMISTRY, ANALYTICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Chemical Metrology","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.25135/jcm.80.2211.2667","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"CHEMISTRY, ANALYTICAL","Score":null,"Total":0}
Phenolic compounds from section Majorana (Mill.) Benth of Origanum L. species extracts via validated LC-MS/MS method
AbstrAbstract: Origanum majorana L., (OM), O. onites L. (OO) and O. syriacum L. (subsp. bevanii (Holmes) Greuter & Burdet) (OS) are belong to Majorana (Mill.) Benth. section of Origanum L. genus. In this study, quantities of some phenolic compounds; gallic acid, syringic acid, p -hydory benzoic acid, caffeic acid, ( E )-ferulic acid, chlorogenic acid, rosmarinic acid, pyrogallol and vanillin; in the chloroform (C), acetone (Ac) and methanol (M) extracts prepared from Origanum species collected from Türkiye were investigated via liquid chromatography and tandem mass spectrometry (LC-MS/MS). The relative standard deviations (RSD) of the phenolics were found as follows; 4.85, 8.39, 4.78, 8.04, 5.21, 5.45, 3.73, 5.47, respectively. Curcumin was used as an internal standard. In the extracts, ( E )-ferulic acid and caffeic acid were found to be the most abundant compounds. O. syriacum was determined as the richest species in terms of phenolic acids.
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