月桂叶提取物制备绿色纳米银的抗菌和催化活性

A. Al-Ghamdi
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引用次数: 8

摘要

在本研究中,月桂提取物(BLE)作为还原剂和封端剂用于合成银纳米颗粒(AgNPs)。使用紫外-可见光谱、傅立叶变换红外光谱(FTIR)、X射线粉末衍射(XRD)、能量分散X射线扫描电子显微镜(SEM-EDX)和透射电子显微镜(TEM)对绿色制备的AgNPs进行了研究。通过从起始溶液到深棕色的颜色变化在环境温度下监测AgNP的形成。研究了绿色合成AgNps的抗菌活性。所用的微生物有大肠杆菌、肺炎克雷伯菌、蜡样芽孢杆菌、金黄色葡萄球菌、乳杆菌和曲霉菌。使用圆盘扩散法测定微生物对六种AgNPs溶液的易感性。研究了所制备的AgNPs(样品,d)对碱性棕色1染料的催化活性。结果表明,AgNPs的特征表面等离子体共振峰出现在415-440nm附近。XRD显示在38.2、44.16、64.24和77.22Ɵ处有峰,与环境温度相比,使用微波固化时这些峰的强度增强。SEM和TEM结果表明,银纳米粒子呈球形,样品的粒径小于34nm。FTIR光谱测量显示有机化合物结合在银纳米颗粒的表面上。随着AgNPs用量的增加和提取物比例的增加,对除外的大多数微生物的最高抗菌活性均增强。制备的AgNPs对碱性棕色1染料的去除表明8小时后染料完全去除。
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Antimicrobial and Catalytic Activities of Green Synthesized Silver Nanoparticles Using Bay Laurel (Laurus nobilis) Leaves Extract
In this study, bay laurel extract (BLE) used as a reducing and capping agent for the synthesis of silver nanoparticles (AgNPs). The green-prepared AgNPs investigated using UV-visible spectroscopy, Fourier-transform infrared spectroscopy (FTIR), X-ray powder diffraction (XRD), Scanning Electron Microscopy with Energy Dispersive X-ray (SEM-EDX) and Transmission electron microscopy (TEM). Formation of AgNPs monitored at ambient temperature by a change in color from the starting solution to dark brown. Green synthesis AgNps were investigated for antimicrobial activity. The microorganisms employed were E. coli, K. pneumoniae, B. cereus, S. aureus, C. lbicans and Aspergillus. The susceptibility of microorganisms against the six AgNPs solutions was determined using the disk diffusion method. The catalytic activity of the prepared AgNPs (sample, d) for basic brown 1 dye was investigated. The results showed the characteristic surface plasmon resonance peak of the AgNPs appeared at approximately 415 - 440 nm. XRD revealed peaks at 38.2, 44.16, 64.24 and 77.22 Ɵ, and the intensity of these peaks enhanced when using microwave curing compared to ambient temperature. SEM and TEM results showed that the silver nano particles have a spherical shape and the particle size for samples is less than 34 nm. FTIR spectroscopy measurements showed the binding of organic compounds on the surface of the silver nanoparticles. Highest antibacterial activity was enhanced with increasing of AgNPs dose and with increasing of extract ration against most of microorganisms except. Removal of basic brown 1 dye by the prepared AgNPs indicated complete dye removal after 8 h.
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