提高klucele/CNC复合材料的机械强度以保护木制文物

Younis, O., El Hadidi, N., D. S., M. M.
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引用次数: 0

摘要

在本研究中,使用浓硫酸(H2 SO4)通过水解程序制备了浓度为2%的纤维素纳米晶体(CNC)。随后制备了不同浓度(10、15、20、30、50%)的CNC/Klucel E纳米复合材料膜。使用X射线衍射(XRD)、扫描电子显微镜(SEM)和拉伸强度测试等不同技术对所获得的薄膜进行了研究和评价。基于所获得的结果,将浓度为20%和30%的薄膜应用于老化木材样品上,以研究这种纳米复合材料对木材不同性能的影响。分别通过拉伸试验、傅立叶变换红外光谱(FT-IR)和颜色变化测量(CIE实验室),从机械性能、化学成分变化和物理外观变化方面研究了这种影响。在Klucel E中添加CNC后,薄膜的拉伸强度在30%的浓度下提高了近70%,使用相同浓度的纳米复合材料后,木材样品的压缩强度显著提高,达到
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ENHANCING THE MECHANICAL STRENGTH OF KLUCEL E/CNC COMPOSITES FOR THE CONSERVATION OF WOODEN ARTIFACTS
: In this research, cellulose nanocrystals (CNC) were prepared with a concentration of 2% through a hydrolysis procedure using conc-entrated sulfuric acid (H 2 SO 4 ). This was followed by the preparation of CNC/Klucel E nanocomposites films with various concentrations (10, 15, 20, 30, 50 %). The obtained films were investigated and evaluated using different techniques such as X-ray diffraction (XRD), Scanning Electron Microscopy (SEM), and tensile strength testing . Based on the results obtained, films with concentrations of 20 and 30 %, which gave the best results, were applied on aged wood specimens in order to study the influence of this nanocomposite on different properties of wood. The influence was studied in terms of mechanical properties, change in chemical composition, and change in physical appearance through tensile tests, Fourier Transform Infrared Spectroscopy (FT-IR) and color change measurements (CIE lab), respectively. The tensile strength of the films was improved after addition of CNC to Klucel E by almost 70% at 30% concentration, and compression strength for wooden samples significantly increased after using the same concentration of the nanocomposite, which reached
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来源期刊
CiteScore
0.40
自引率
50.00%
发文量
12
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