摘要以水为溶剂,用微波法提取菠萝蜜木渣中的天然染料

S. Gala, M. Mahfud, S. Sumarno, L. Qadariyah
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引用次数: 3

摘要

目前,对天然染料的探索日益活跃和发展,特别是从不同植物物种中寻找天然染料来源,以及开发用于纺织的天然染料提取工艺技术。在此过程中,天然染料的提取是通过传统的方法完成的,需要很长时间和大量的溶剂。因此,它是一种必要的替代使用的“绿色技术”在其使用是经济的。本研究通过研究微波提取菠萝蜜木渣所需的提取时间,并与常规方法(热回流提取)进行比较,得出最佳得率。这两种方法都使用水溶剂。对微波辅助提取,最佳提取时间为30 min,得率为3.14%(微波功率400瓦,料溶剂比0.02 g/mL)。热回流法的最佳提取时间为180 min,得率为3.50%。菠萝蜜木渣中所含的色素可分为单宁、黄酮类和醌类。采用傅里叶变换红外光谱法对提取染料中的主要化学基团进行了鉴定。描述微波萃取和常规萃取的效果,用扫描电子显微镜观察固体表面材料的结构损伤。进一步测试其在织物染色上的应用。
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THE EXTRACTION OF NATURAL DYES FROM JACKFRUIT WOOD WASTE (Artocarpus Heterophyllus Lamk) WITH WATER SOLVENT BY USING THE MICROWAVE METHOD
Currently, exploration of natural dyes is increasingly being activated and developed, especially to find natural sources of dyes from different plant species and also to develop natural dyestuff extraction process technology for textile applications. During this natural dye extraction process is done by conventional methods that require a long time and a large amount of solvent. Therefore, it is a necessary alternative to the use of "green techniques" are economical in its use. In this research, extraction of Jackfruit wood waste with the microwave by studying the extraction time required to produce the optimum yield and comparing with the conventional method (heat-reflux extraction). Both of these methods use water solvent. On the microwave-assisted extraction, the optimum extraction time at 30 minutes with the acquisition yield of 3.14% (microwave power 400 watt, the ratio of material to solvent 0.02 g/mL). whereas extraction with heat-reflux method showed the optimum extraction time of 180 minutes with a yield of 3.50%. Identification of groups of pigments contained in the Jackfruit wood waste is known categories tannins, flavonoids, and quinones. Fourier Transform Infrared Spectroscopy was used to identify the major chemical groups in the extracted dye. Description of the effects of extraction with microwave and conventional, structural damage shown in a solid surface material using by Scanning Electron Microscopy. Further, to test the application on the fabric dyeing.
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