椰子油固体脂肪含量静态与动态分析的比较

IF 0.5 Q4 ENGINEERING, CHEMICAL Hungarian Journal of Industry and Chemistry Pub Date : 2018-12-01 DOI:10.1515/hjic-2018-0015
Vinod Dhaygude, A. Soós, I. Zeke, L. Somogyi
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引用次数: 1

摘要

摘要本工作的目的是通过差示扫描量热法(DSC)和脉冲核磁共振(pNMR)的结果来比较两种椰子油及其混合物的物理和热特性。制备由不同比例组成的脂肪混合物(完全氢化椰子油/未氢化椰子油:25/75、50/50和75/25),并检查固体脂肪含量。通过pNMR测定样品的固体脂肪含量作为温度的函数。DSC技术通过连续测量不同温度下的熔融热来确定固体脂肪指数。DSC计算脂肪样品中固体的实际含量,以及它在加热或冷却过程中的变化。通过焓的相关性来构建特征曲线。基于我们的结果,很明显,DSC和pNMR技术都提供了关于脂肪中固体脂肪含量的非常实用和有用的信息。DSC是动态的,pNMR是静态的。观察到样品的固体脂肪指数值的差异,这可能是由于两种技术之间的根本差异。食品制造商可以使用这些数据来优化改性椰子油和用椰子油强化的食品的加工条件。
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Comparison Between Static and Dynamic Analyses of The Solid Fat Content of Coconut Oil
Abstract The objective of this work was to compare the physical and thermal characteristics of two coconut oils and their blends which were observed by the results of differential scanning calorimetry (DSC) and pulsed nuclear magnetic resonance (pNMR). Fat blends composed of different ratios (fully hydrogenated coconut oil / non-hydrogenated coconut oil: 25/75, 50/50 and 75/25) were prepared and examined for solid fat content. The solid fat content of samples was determined as a function of temperature by pNMR. The DSC technique determines the solid fat index by measuring the heat of fusion successively at different temperatures. DSC calculates the actual content of solids in fat samples and how it changes throughout the duration of heating or cooling. A characteristic curve is constructed by the correlation of enthalpies. Based on our results, it is clear that both DSC and pNMR techniques provide very practical and useful information on the solid fat content of fats. DSC is dynamic and pNMR is static. A difference in the values of the solid fat indexes of samples was observed which may be due to a fundamental difference between the two techniques. These data can be used by food manufacturers to optimize processing conditions for modified coconut oil and food products fortified with coconut oil.
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来源期刊
自引率
50.00%
发文量
9
审稿时长
6 weeks
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