{"title":"大Sc数范围内叶轮叶顶与表面距离对搅拌容器内局部电极传质的影响","authors":"S. Yapici, İlhan Altay","doi":"10.1080/00194506.2022.2059020","DOIUrl":null,"url":null,"abstract":"ABSTRACT\n Stirred vessels are encountered in a wide scale of applications from bench to industrial processes, and the knowledge of the heat/mass transfer rates in these vessels is required for their design, operation and control. This work submits an investigation on the mass transfer to a small circular surface immersed in a stirred vessel in the parameter ranges of 267 < Re < 9437, 1473 < Sc < 61,422, and 0.022 < x/dK < 0.22 for the distance between the impeller blade tip and the transfer surface. The Reynolds number was based on the impeller diameter. The electrochemical limiting diffusion current technique having a potassium ferri-/ferrocyanide system was applied for mass transfer coefficient measurements. Aqueous glycerine solutions were prepared to attain a wide range of Sc numbers. The rate of mass transfer is enhanced with increasing rotation rate, decreasing blade tip-to-electrode surface distance, and decreasing glycerine concentration. The experimental data were well correlated by the relation . GRAPHICAL ABSTRACT","PeriodicalId":13430,"journal":{"name":"Indian Chemical Engineer","volume":null,"pages":null},"PeriodicalIF":0.9000,"publicationDate":"2022-04-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Effect of distance between impeller blade tip and surface on mass transfer to a local electrode in a stirred vessel in a wide range of Sc number\",\"authors\":\"S. Yapici, İlhan Altay\",\"doi\":\"10.1080/00194506.2022.2059020\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"ABSTRACT\\n Stirred vessels are encountered in a wide scale of applications from bench to industrial processes, and the knowledge of the heat/mass transfer rates in these vessels is required for their design, operation and control. This work submits an investigation on the mass transfer to a small circular surface immersed in a stirred vessel in the parameter ranges of 267 < Re < 9437, 1473 < Sc < 61,422, and 0.022 < x/dK < 0.22 for the distance between the impeller blade tip and the transfer surface. The Reynolds number was based on the impeller diameter. The electrochemical limiting diffusion current technique having a potassium ferri-/ferrocyanide system was applied for mass transfer coefficient measurements. Aqueous glycerine solutions were prepared to attain a wide range of Sc numbers. The rate of mass transfer is enhanced with increasing rotation rate, decreasing blade tip-to-electrode surface distance, and decreasing glycerine concentration. The experimental data were well correlated by the relation . GRAPHICAL ABSTRACT\",\"PeriodicalId\":13430,\"journal\":{\"name\":\"Indian Chemical Engineer\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.9000,\"publicationDate\":\"2022-04-06\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Indian Chemical Engineer\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1080/00194506.2022.2059020\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"ENGINEERING, CHEMICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Indian Chemical Engineer","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1080/00194506.2022.2059020","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"ENGINEERING, CHEMICAL","Score":null,"Total":0}
Effect of distance between impeller blade tip and surface on mass transfer to a local electrode in a stirred vessel in a wide range of Sc number
ABSTRACT
Stirred vessels are encountered in a wide scale of applications from bench to industrial processes, and the knowledge of the heat/mass transfer rates in these vessels is required for their design, operation and control. This work submits an investigation on the mass transfer to a small circular surface immersed in a stirred vessel in the parameter ranges of 267 < Re < 9437, 1473 < Sc < 61,422, and 0.022 < x/dK < 0.22 for the distance between the impeller blade tip and the transfer surface. The Reynolds number was based on the impeller diameter. The electrochemical limiting diffusion current technique having a potassium ferri-/ferrocyanide system was applied for mass transfer coefficient measurements. Aqueous glycerine solutions were prepared to attain a wide range of Sc numbers. The rate of mass transfer is enhanced with increasing rotation rate, decreasing blade tip-to-electrode surface distance, and decreasing glycerine concentration. The experimental data were well correlated by the relation . GRAPHICAL ABSTRACT