甜橙皮精油提取率及抗氧化性能的比较研究

O. Olabinjo, A.L.M. Oliveira
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引用次数: 1

摘要

文章历史:收到时间:2019年9月25日接受时间:2020年6月16日该研究使用加压液体提取(PLE)、索氏提取(Sox)和加氢蒸馏(HD)评估了甜橙皮精油(EO)的提取率和抗氧化潜力。用2,2-二苯基-1-丙酰基-肼(DPPH)和2,2-叠氮基双(3-乙基苯并噻唑啉-6磺酸酯)自由基(ABTS•+)对提取物进行了抗氧化性能研究。PLE和索氏提取的精油分别通过薄层色谱和化学分析显示出额外的多酚化合物和单宁。加氢蒸馏表明,与PLE和Soxhlet的其他精油相比,不含单宁和多酚的纯精油具有最高的ABTS活性。采用气相色谱-质谱法(GC-MS)对纯精油的主要化学成分进行了鉴定,包括柠檬烯(90.72%)、月桂烯(2.82%)和乙酸辛醇(1.24%)。
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Comparative study of extraction yield and antioxidant property of sweet orange peels (Citrus Sinesis) essential oil
Article history: Received: September 25, 2019 Accepted: June 16, 2020 The research evaluates the extraction yield and antioxidant potentials of essential oil (EO) of sweet orange peels using pressurized liquid extraction (PLE), Soxhlet (Sox) and hydro distillation (HD). The extracts were investigated to find out the antioxidant properties using 2, 2 -diphenyl-1picryl-hydrazyl (DPPH) and 2, 2 azino-bis (3-ethylbenzothiazoline-6sulfonate) radical (ABTS•+). PLE and Soxhlet extracted essential oil showed additional polyphenol compounds and tannins using thin layer chromatogram (TLC) and chemical analyses, respectively. Hydrodistillation indicating a pure essential oil without identified tannins and polyphenols with the highest ABTS activity compared to other produced essential oils of PLE and Soxhlet. The major chemical constituents of the pure essential oil were identified by gas chromatography-mass spectrometry (GC-MS) and they include limonene (90.72%), myrcene (2.82%) and octanol acetate (1.24%). PLE had moderate high yield within short extraction time and the highest antioxidant (DPPH) and can be adjusted to individual materials to maximize the extraction yield and antioxidant property.
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发文量
16
审稿时长
12 weeks
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