{"title":"(Al2O3)纳米粒子的加入对Bi2Ba2Ca2Cu3O10“+δ”超导体高温结构和电性能的影响","authors":"Fouad Kamal Tawfeeq Alsumaidaei, H. Mohammed","doi":"10.32894/kujss.2020.167506","DOIUrl":null,"url":null,"abstract":"To enhancement the superconductor structural characteristics, nanoparticles of the Al 2O3 were added to the samples under study. The Samples of high temperature superconductors 1 X (Bi2Ba2Ca2Cu3O10+ ) + X(Al2O3) with X= (0-0.9) were prepared by solid state reaction method under hydraulic pressure 8 ton/cm 2 and annealing temperature 800. Electrical properties of the samples showed that Tc increases from 12 6 K to 139 K, and also oxygen content in samples increased with increasing X values from 0 to 0.5, while T c d creased less than 77 K with increasing X at values more than 0.5. In Structural properties, the X -ray diffraction of the samples showed orthorhombic phase wi th a=4.286A, b=5.4184A, c=35.3528A at X=0, while c-value is increased to 35.9848A at X=0.5. AFM results shows that the average grain size of the best sample was 47.67 nm at X=0.5. SEM it showed that there are dark regions related to the heav ier elements, such as Bi and Cu , and light regi ons related to lighter elements , uch as Ba and Ca , depending on atomic weights","PeriodicalId":34247,"journal":{"name":"mjl@ jm`@ krkwk ldrst l`lmy@","volume":" ","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2020-12-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"The Effect of Addition of (Al2O3) Nano Particles on Structural and Electrical Properties of Bi2Ba2Ca2Cu3O10\\\" +δ\\\" Superconductors at High Temperature\",\"authors\":\"Fouad Kamal Tawfeeq Alsumaidaei, H. Mohammed\",\"doi\":\"10.32894/kujss.2020.167506\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"To enhancement the superconductor structural characteristics, nanoparticles of the Al 2O3 were added to the samples under study. The Samples of high temperature superconductors 1 X (Bi2Ba2Ca2Cu3O10+ ) + X(Al2O3) with X= (0-0.9) were prepared by solid state reaction method under hydraulic pressure 8 ton/cm 2 and annealing temperature 800. Electrical properties of the samples showed that Tc increases from 12 6 K to 139 K, and also oxygen content in samples increased with increasing X values from 0 to 0.5, while T c d creased less than 77 K with increasing X at values more than 0.5. In Structural properties, the X -ray diffraction of the samples showed orthorhombic phase wi th a=4.286A, b=5.4184A, c=35.3528A at X=0, while c-value is increased to 35.9848A at X=0.5. AFM results shows that the average grain size of the best sample was 47.67 nm at X=0.5. SEM it showed that there are dark regions related to the heav ier elements, such as Bi and Cu , and light regi ons related to lighter elements , uch as Ba and Ca , depending on atomic weights\",\"PeriodicalId\":34247,\"journal\":{\"name\":\"mjl@ jm`@ krkwk ldrst l`lmy@\",\"volume\":\" \",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2020-12-31\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"mjl@ jm`@ krkwk ldrst l`lmy@\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.32894/kujss.2020.167506\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"mjl@ jm`@ krkwk ldrst l`lmy@","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.32894/kujss.2020.167506","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
The Effect of Addition of (Al2O3) Nano Particles on Structural and Electrical Properties of Bi2Ba2Ca2Cu3O10" +δ" Superconductors at High Temperature
To enhancement the superconductor structural characteristics, nanoparticles of the Al 2O3 were added to the samples under study. The Samples of high temperature superconductors 1 X (Bi2Ba2Ca2Cu3O10+ ) + X(Al2O3) with X= (0-0.9) were prepared by solid state reaction method under hydraulic pressure 8 ton/cm 2 and annealing temperature 800. Electrical properties of the samples showed that Tc increases from 12 6 K to 139 K, and also oxygen content in samples increased with increasing X values from 0 to 0.5, while T c d creased less than 77 K with increasing X at values more than 0.5. In Structural properties, the X -ray diffraction of the samples showed orthorhombic phase wi th a=4.286A, b=5.4184A, c=35.3528A at X=0, while c-value is increased to 35.9848A at X=0.5. AFM results shows that the average grain size of the best sample was 47.67 nm at X=0.5. SEM it showed that there are dark regions related to the heav ier elements, such as Bi and Cu , and light regi ons related to lighter elements , uch as Ba and Ca , depending on atomic weights