Masation法和Sonization法提取芒果叶黄酮的比较:溶剂配比的影响

Q4 Chemical Engineering ASEAN Journal of Chemical Engineering Pub Date : 2022-12-29 DOI:10.22146/ajche.74204
A. Sari, Nur Layli Amanah, Awalia Wardatullathifah, A. Nugroho
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引用次数: 2

摘要

芒果叶提取物已被证明含有作为抗氧化剂的类黄酮。对传统浸渍法和超声波法提取芒果叶黄酮进行了比较研究。采用不同比例的乙醇和丙酮作为溶剂(1:5,1:10和1:15)。超声波处理过程使用40℃的超声波清洗浴,只需30分钟,而在室温下浸泡过程需要36小时。用氯化铝(AlCl3)比色法测定黄酮类化合物,结果表明丙酮比乙醇具有更大的溶剂力。根据本研究,浸渍和超声程序的最佳比例分别为1:10和1:15。浸渍工艺的最佳浸出量为0.186 mgQE/g干叶。同时,采用丙酮溶剂比为1:15的超声法,发现黄酮类成分的最高浓度为0.143 mgQE/g,干燥时间缩短了54倍。
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Comparison of Maseration and Sonication Method on Flavonoid Extraction from Mango Leaves: Effect of Solvent Ratio
Mango leaf extract has proven to contain flavonoids that serve as antioxidants. In this study, a comparison between traditional maceration and sonication on flavonoid extraction from mango leaf was investigated. The various ratios of ethanol and acetone were utilized as solvents (1:5, 1:10, and 1:15). The sonication process, which uses an ultrasonic cleaning bath set at 40 oC, takes 30 minutes as contrasted to the maceration procedure of 36 hours treatment at room temperature. The flavonoid test using aluminum (III) chloride (AlCl3) colorimetric technique shows that acetone provides greater solvent power than ethanol. According to this study, the optimal ratios for the maceration and sonication procedures are 1:10 and 1:15, respectively. The maceration process resulted in the optimum extract of 0.186 mgQE/g dry leaves. Meanwhile, using a 1:15 acetone solvent ratio and the sonication method, the highest concentration of flavonoid components was discovered, reaching 0.143 mgQE/g dry material with 54 times shorter time.
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来源期刊
ASEAN Journal of Chemical Engineering
ASEAN Journal of Chemical Engineering Chemical Engineering-Chemical Engineering (all)
CiteScore
1.00
自引率
0.00%
发文量
15
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