利用稻壳二氧化硅和石灰石碳酸钙合成白色矿物三氧化物骨料(WMTA)

Anwar Jaman, Muhammad Ulin Nuha Aba, O. A. Widyayanti
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引用次数: 0

摘要

采用从稻壳灰和碳酸钙石灰石中提取的二氧化硅为原料,制备了白色矿物三氧化物骨料(WMTA)。这项研究是通过在700°C下煅烧稻壳灰3小时开始的。使用2M NaOH并加入HCl进行二氧化硅提取。使用去离子水洗涤提取物沉淀物。碳酸钙由石灰石使用1M HNO3和NH3制备,并继续碳酸化。WMTA是通过混合SiO2、CaCO3和Al2O3来生产的。将混合物用去离子水均匀化并加热,然后在1000°C的温度下煅烧制成颗粒,并添加煅烧产物Bi2O3。使用TGA/DSC、FTIR和XRD表征的合成WMTA显示出Ca3SiO5、Ca2SiO4和Ca3Al2O6相的存在,其类似于ProRoot的WMTA。
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Synthesis of White Mineral Trioxide Aggregate (WMTA) Using Silica from Rice Husk and Calcium Carbonate from Limestone
White Mineral Trioxide Aggregate (WMTA) was produced using silica as the initial material extracted from rice husk ash and calcium carbonate limestone. This research was initiated by calcinating rice husk ash at 700°C for 3 hours. Silica extraction was performed using 2 M NaOH and added HCl. The extract precipitate was washed using deionized water. Calcium carbonate was made from limestone using 1 M HNO3 and NH3 and continued with carbonation. WMTA was produced by mixing SiO2, CaCO3, and Al2O3. The mixture was homogenized with deionized water and heated, then pellets calcined made at a temperature of 1000°C, and calcination products were added Bi2O3. Synthesized WMTA characterized using TGA/DSC, FTIR, and XRD showed the presence of Ca3SiO5, Ca2SiO4, and Ca3Al2O6 phases, which were like ProRoot’s WMTA.
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发文量
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审稿时长
17 weeks
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