A. Karthikeyan, J. Suresh, K. Balaji, S. Anandhakumar, A. Arun
{"title":"三嗪基羟基查尔酮纳米金属配合物的合成、表征及抗氧化性能","authors":"A. Karthikeyan, J. Suresh, K. Balaji, S. Anandhakumar, A. Arun","doi":"10.1080/23080477.2022.2074660","DOIUrl":null,"url":null,"abstract":"ABSTRACT In the present investigation, novel triazine-based chalcone ligand (1-(2,4-dihydroxyphenyl)-3-(4-((4-((4-nitrophenyl)amino)-6-phenoxy-1,3,5-triazin-2-yl)oxy)phenyl) prop-2-en-1-one) (DNPP) is synthesized and used in metal complexes synthesis which contains iron, copper, nickel, and zinc. 1H NMR and IR spectrum of DNPP confirms the formation of the product. UV-Visible spectrum shows a peak around 400–500 nm for d-d transition. SEM with EDX shows the metal complexes is in crystalline state with the size in the range of 20–50 nm. TGA analysis shows the synthesized compound is highly stable and the residue content confirms the presence of metal in the molecular structure. Antioxidant were found out to be <50 μg/ml. Graphical Abstract","PeriodicalId":53436,"journal":{"name":"Smart Science","volume":"11 1","pages":"192 - 203"},"PeriodicalIF":2.4000,"publicationDate":"2022-05-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Synthesis, characterization and antioxidant property of nano-scaled metal complexes of triazine based hydroxy chalcone\",\"authors\":\"A. Karthikeyan, J. Suresh, K. Balaji, S. Anandhakumar, A. Arun\",\"doi\":\"10.1080/23080477.2022.2074660\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"ABSTRACT In the present investigation, novel triazine-based chalcone ligand (1-(2,4-dihydroxyphenyl)-3-(4-((4-((4-nitrophenyl)amino)-6-phenoxy-1,3,5-triazin-2-yl)oxy)phenyl) prop-2-en-1-one) (DNPP) is synthesized and used in metal complexes synthesis which contains iron, copper, nickel, and zinc. 1H NMR and IR spectrum of DNPP confirms the formation of the product. UV-Visible spectrum shows a peak around 400–500 nm for d-d transition. SEM with EDX shows the metal complexes is in crystalline state with the size in the range of 20–50 nm. TGA analysis shows the synthesized compound is highly stable and the residue content confirms the presence of metal in the molecular structure. Antioxidant were found out to be <50 μg/ml. Graphical Abstract\",\"PeriodicalId\":53436,\"journal\":{\"name\":\"Smart Science\",\"volume\":\"11 1\",\"pages\":\"192 - 203\"},\"PeriodicalIF\":2.4000,\"publicationDate\":\"2022-05-18\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Smart Science\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1080/23080477.2022.2074660\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MULTIDISCIPLINARY SCIENCES\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Smart Science","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1080/23080477.2022.2074660","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MULTIDISCIPLINARY SCIENCES","Score":null,"Total":0}
Synthesis, characterization and antioxidant property of nano-scaled metal complexes of triazine based hydroxy chalcone
ABSTRACT In the present investigation, novel triazine-based chalcone ligand (1-(2,4-dihydroxyphenyl)-3-(4-((4-((4-nitrophenyl)amino)-6-phenoxy-1,3,5-triazin-2-yl)oxy)phenyl) prop-2-en-1-one) (DNPP) is synthesized and used in metal complexes synthesis which contains iron, copper, nickel, and zinc. 1H NMR and IR spectrum of DNPP confirms the formation of the product. UV-Visible spectrum shows a peak around 400–500 nm for d-d transition. SEM with EDX shows the metal complexes is in crystalline state with the size in the range of 20–50 nm. TGA analysis shows the synthesized compound is highly stable and the residue content confirms the presence of metal in the molecular structure. Antioxidant were found out to be <50 μg/ml. Graphical Abstract
期刊介绍：
Smart Science (ISSN 2308-0477) is an international, peer-reviewed journal that publishes significant original scientific researches, and reviews and analyses of current research and science policy. We welcome submissions of high quality papers from all fields of science and from any source. Articles of an interdisciplinary nature are particularly welcomed. Smart Science aims to be among the top multidisciplinary journals covering a broad spectrum of smart topics in the fields of materials science, chemistry, physics, engineering, medicine, and biology. Smart Science is currently focusing on the topics of Smart Manufacturing (CPS, IoT and AI) for Industry 4.0, Smart Energy and Smart Chemistry and Materials. Other specific research areas covered by the journal include, but are not limited to: 1. Smart Science in the Future 2. Smart Manufacturing: -Cyber-Physical System (CPS) -Internet of Things (IoT) and Internet of Brain (IoB) -Artificial Intelligence -Smart Computing -Smart Design/Machine -Smart Sensing -Smart Information and Networks 3. Smart Energy and Thermal/Fluidic Science 4. Smart Chemistry and Materials
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