{"title":"用于NO2气体检测的硅沉积锰掺杂氧化锌薄膜","authors":"N. Abood, P. Sable, G. Dharne","doi":"10.1080/01411594.2023.2179921","DOIUrl":null,"url":null,"abstract":"ABSTRACT The structural, optical and gas detection characteristics of Mn-doped ZnO thin films synthesised by the Successive Ionic Layer Adsorption and Reaction (SILAR) process with varied doping concentrations (4, 6 and 8%) were examined. X-ray diffraction data was used to investigate the structural properties and confirm the hexagonal wurtzite crystal structure. The surface morphology and the existence of all elements were verified using a field emission scanning electron microscope and energy dispersive X-ray spectroscopy, respectively. To explore the vibrational bands present in Mn-doped ZnO films, we used FTIR spectra at ambient temperature. Ultraviolet-visible analysis reveals the absorption edge, which is found in the ultraviolet area, with a minor shift towards high wave length, whereas the energy bandgap decreases as Mn concentrations increase. At 200°C operating temperature, the gas sensing properties of Zn0.92Mn0.08O showed good sensitivity, selectivity and shorter response time when compared to other prepared films.","PeriodicalId":19881,"journal":{"name":"Phase Transitions","volume":"96 1","pages":"274 - 289"},"PeriodicalIF":1.3000,"publicationDate":"2023-02-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"SILAR-deposited manganese doped zinc oxide thin films for NO2 gas detection applications\",\"authors\":\"N. Abood, P. Sable, G. Dharne\",\"doi\":\"10.1080/01411594.2023.2179921\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"ABSTRACT The structural, optical and gas detection characteristics of Mn-doped ZnO thin films synthesised by the Successive Ionic Layer Adsorption and Reaction (SILAR) process with varied doping concentrations (4, 6 and 8%) were examined. X-ray diffraction data was used to investigate the structural properties and confirm the hexagonal wurtzite crystal structure. The surface morphology and the existence of all elements were verified using a field emission scanning electron microscope and energy dispersive X-ray spectroscopy, respectively. To explore the vibrational bands present in Mn-doped ZnO films, we used FTIR spectra at ambient temperature. Ultraviolet-visible analysis reveals the absorption edge, which is found in the ultraviolet area, with a minor shift towards high wave length, whereas the energy bandgap decreases as Mn concentrations increase. At 200°C operating temperature, the gas sensing properties of Zn0.92Mn0.08O showed good sensitivity, selectivity and shorter response time when compared to other prepared films.\",\"PeriodicalId\":19881,\"journal\":{\"name\":\"Phase Transitions\",\"volume\":\"96 1\",\"pages\":\"274 - 289\"},\"PeriodicalIF\":1.3000,\"publicationDate\":\"2023-02-28\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Phase Transitions\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1080/01411594.2023.2179921\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"CRYSTALLOGRAPHY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Phase Transitions","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1080/01411594.2023.2179921","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"CRYSTALLOGRAPHY","Score":null,"Total":0}
SILAR-deposited manganese doped zinc oxide thin films for NO2 gas detection applications
ABSTRACT The structural, optical and gas detection characteristics of Mn-doped ZnO thin films synthesised by the Successive Ionic Layer Adsorption and Reaction (SILAR) process with varied doping concentrations (4, 6 and 8%) were examined. X-ray diffraction data was used to investigate the structural properties and confirm the hexagonal wurtzite crystal structure. The surface morphology and the existence of all elements were verified using a field emission scanning electron microscope and energy dispersive X-ray spectroscopy, respectively. To explore the vibrational bands present in Mn-doped ZnO films, we used FTIR spectra at ambient temperature. Ultraviolet-visible analysis reveals the absorption edge, which is found in the ultraviolet area, with a minor shift towards high wave length, whereas the energy bandgap decreases as Mn concentrations increase. At 200°C operating temperature, the gas sensing properties of Zn0.92Mn0.08O showed good sensitivity, selectivity and shorter response time when compared to other prepared films.
期刊介绍：
Phase Transitions is the only journal devoted exclusively to this important subject. It provides a focus for papers on most aspects of phase transitions in condensed matter. Although emphasis is placed primarily on experimental work, theoretical papers are welcome if they have some bearing on experimental results. The areas of interest include:
-structural phase transitions (ferroelectric, ferroelastic, multiferroic, order-disorder, Jahn-Teller, etc.) under a range of external parameters (temperature, pressure, strain, electric/magnetic fields, etc.)
-geophysical phase transitions
-metal-insulator phase transitions
-superconducting and superfluid transitions
-magnetic phase transitions
-critical phenomena and physical properties at phase transitions
-liquid crystals
-technological applications of phase transitions
-quantum phase transitions
Phase Transitions publishes both research papers and invited articles devoted to special topics. Major review papers are particularly welcome. A further emphasis of the journal is the publication of a selected number of small workshops, which are at the forefront of their field.
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