开发了基于MW在制造CNF中实施的更环保方法

Loai Aljerf, Rim Nadra
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引用次数: 87

摘要

这项研究是首次使用微波(MW)与辅助化学气相沉积(CVD)相结合在短周期热反应中产生均匀碳纳米纤维(CNFs)的试验。结果证实,这些材料具有高度有序的热解石墨性质。获得具有均匀直径(80-150nm)和长纤维(0.82-1.75μm)的CNFs。SEM和TEM评估显示,断裂表面的损伤相对较小,TGA显示CNFs在热分解过程中变化不大。“固体”CNFs表现出明显的无序、结晶和弯曲石墨片性质。所制备的CNT表现出良好的MW吸收性能和优异的性能,这可能是由于介电型吸收和多反射MW的干扰的结合。这种增强使新型制造的CNFs的纯度达到97%。因此,我们推荐我们的绿色纳米产品用于能源、制药、化妆品、纺织、传感器、电子、车辆以及量子点(QD)和荧光C点等行业。
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Developed greener method based on MW implementation in manufacturing CNFs
This study comes as the first trial that uses microwave (MW) in combination with assisted chemical vapour deposition (CVD) to generate homogeneous carbon nanofibers (CNFs) at short period thermal reaction. The outcomes confirmed that these materials are of highly-ordered pyrolitic graphite nature. CNFs were obtained having uniform diameters (80-150 nm) and long fibres (0.82-1.75 μm). SEM and TEM evaluations revealed relatively less damage in fractured surfaces and the TGA exhibited insignificant change of CNFs during thermal decomposition. The 'solid' CNFs showed clear properties as disorder, crystalline, and bent graphitic sheets. The as-prepared CNTs demonstrated good MW-absorption properties with superior performance which could be due to the combination of the dielectric-type absorption and the interference of multi-reflected MW. This enhancement gave 97% purity of the novel manufactured CNFs. Therefore, we recommend our greener nanoproducts for industries as energy, pharmaceutical, cosmetics, textile, sensors, electronics, vehicles, and both of quantum dots (QD) and fluorescent C-dots.
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来源期刊
International Journal of Nanomanufacturing
International Journal of Nanomanufacturing Engineering-Industrial and Manufacturing Engineering
CiteScore
0.60
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0.00%
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