α和β硅灰石生物陶瓷在模拟体液中的生物活性评价

L. A. Núñez-Rodríguez, M. A. Encinas-Romero, A. Gómez-Álvarez, J. Valenzuela-García, Guillermo C. Tiburcio-Munive
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引用次数: 13

摘要

采用烧结法制备了致密的天然硅灰石生物陶瓷(CaSiO3),通过改变压制载荷和烧结温度,获得了硅灰石不同相、不同物性的材料。采用tg - dta、XRD、FT-IR、SEM-EDS、TEM和XPS等技术对产物进行了表征。结果表明,硅灰石存在β-硅灰石和α-硅灰石两种多晶相,β相向α相转变温度约为1250℃。将这些材料在模拟体液(SBF)中浸泡1、2和3周,研究其溶解度和生物活性。分析了硅灰石不同相对Ca和Si溶解度的影响,以及在SBF溶液中硅灰石材料表面生成“新形成的磷灰石”层的能力。
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Evaluation of Bioactive Properties of α and β Wollastonite Bioceramics Soaked in a Simulated Body Fluid
Dense natural wollastonite bioceramics (CaSiO3) were prepared by a sintering method, varying the pressing load and sintering temperature, in order to obtain different phases of wollastonite, and different physical properties in the materials. The products were characterized by TGA-DTA, XRD, FT-IR, SEM-EDS, TEM and XPS techniques. The results indicate the presence of two polymorphic phases of wollastonite, the β-wollastonite and α-wollastonite with a transition temperature of the β phase to α phase at approximately 1250℃. These materials were soaked in a simulated body fluid (SBF) during 1, 2 and 3 weeks, to study their solubility and bioactivity. The effect of different wollastonite phases on the solubility of Ca and Si, as well as the capacity of producing layers of “newly formed apatite” on the surfaces of these materials in SBF solution were analyzed.
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