M. Mališová, M. Horňáček, P. Hudec, J. Mikulec, V. Jorík, E. Hájeková
{"title":"水滑石制备条件对其理化性能的影响","authors":"M. Mališová, M. Horňáček, P. Hudec, J. Mikulec, V. Jorík, E. Hájeková","doi":"10.2478/acs-2019-0017","DOIUrl":null,"url":null,"abstract":"Abstract The aim of the research was to prepare and characterize hydrotalcite synthesized under different preparation conditions. The most common hydrotalcite preparation is the co-precipiaton method. The preparation process strongly influences the catalytic properties of hydrotalcite; therefore, optimal conditions have to be determined. During the study, seven samples of the catalyst were prepared in the pH range from 8 to 12 and the synthesis temperature range from 25 to 55 °C. Based on several catalyst properties, optimal synthesis pH 10 was found. Ideal temperature of the preparation was determined to be 35 °C, but the temperature does not have a significant effect on the catalyst properties.","PeriodicalId":7088,"journal":{"name":"Acta Chimica Slovaca","volume":"12 1","pages":"119 - 126"},"PeriodicalIF":0.9000,"publicationDate":"2019-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"2","resultStr":"{\"title\":\"Influence of hydrotalcite preparation conditions on its physico-chemical properties\",\"authors\":\"M. Mališová, M. Horňáček, P. Hudec, J. Mikulec, V. Jorík, E. Hájeková\",\"doi\":\"10.2478/acs-2019-0017\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Abstract The aim of the research was to prepare and characterize hydrotalcite synthesized under different preparation conditions. The most common hydrotalcite preparation is the co-precipiaton method. The preparation process strongly influences the catalytic properties of hydrotalcite; therefore, optimal conditions have to be determined. During the study, seven samples of the catalyst were prepared in the pH range from 8 to 12 and the synthesis temperature range from 25 to 55 °C. Based on several catalyst properties, optimal synthesis pH 10 was found. Ideal temperature of the preparation was determined to be 35 °C, but the temperature does not have a significant effect on the catalyst properties.\",\"PeriodicalId\":7088,\"journal\":{\"name\":\"Acta Chimica Slovaca\",\"volume\":\"12 1\",\"pages\":\"119 - 126\"},\"PeriodicalIF\":0.9000,\"publicationDate\":\"2019-04-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"2\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Acta Chimica Slovaca\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.2478/acs-2019-0017\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"CHEMISTRY, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Acta Chimica Slovaca","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2478/acs-2019-0017","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
Influence of hydrotalcite preparation conditions on its physico-chemical properties
Abstract The aim of the research was to prepare and characterize hydrotalcite synthesized under different preparation conditions. The most common hydrotalcite preparation is the co-precipiaton method. The preparation process strongly influences the catalytic properties of hydrotalcite; therefore, optimal conditions have to be determined. During the study, seven samples of the catalyst were prepared in the pH range from 8 to 12 and the synthesis temperature range from 25 to 55 °C. Based on several catalyst properties, optimal synthesis pH 10 was found. Ideal temperature of the preparation was determined to be 35 °C, but the temperature does not have a significant effect on the catalyst properties.