由取代的磷酸三钙Ca3(PO4)2制成并用硅酸盐玻璃纤维增强的磷酸钙-刷石水泥

IF 0.8 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Materials Science-medziagotyra Pub Date : 2023-02-21 DOI:10.31044/1684-579x-2023-0-5-19-27
Sharifjon A Musoev, A. Knotko, Y. Filippov
{"title":"由取代的磷酸三钙Ca3(PO4)2制成并用硅酸盐玻璃纤维增强的磷酸钙-刷石水泥","authors":"Sharifjon A Musoev, A. Knotko, Y. Filippov","doi":"10.31044/1684-579x-2023-0-5-19-27","DOIUrl":null,"url":null,"abstract":"The reinforcement of reaction hardening phosphate materials (phosphate cements) for bone implants, based on isomorphically cation- (Na+, K+) and anion- (SiO44-, SO42-) substituted tricalcium phosphate (β and α-TCP, Ca3(PO4)2), that are reinforced with silicate (basalt-based) fiberglass, is considered. The obtained materials were characterized by the XRD and SEM methods, mechanical compression tests were carried out, the setting times of cements were determined, changes in the pH of the aqueous medium in contact with the cements under study were measured. Microstructure analysis has been shown that the surface of the reinforcing fiber in contact with the matrix of hardening cement is partially corroded with the formation of phosphate microparticles on it. By pH-metry it was found that the samples during prolonged contact with water do not significantly change the pH value of the aquatic environment, which remains in the nearly neutral range from 5 to 7.5, favorable for further biological tests.","PeriodicalId":18298,"journal":{"name":"Materials Science-medziagotyra","volume":null,"pages":null},"PeriodicalIF":0.8000,"publicationDate":"2023-02-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Calcium phosphate brushite cements made from substituted tricalcium phosphate Ca3(PO4)2 and reinforced with silicate glass fiber\",\"authors\":\"Sharifjon A Musoev, A. Knotko, Y. Filippov\",\"doi\":\"10.31044/1684-579x-2023-0-5-19-27\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The reinforcement of reaction hardening phosphate materials (phosphate cements) for bone implants, based on isomorphically cation- (Na+, K+) and anion- (SiO44-, SO42-) substituted tricalcium phosphate (β and α-TCP, Ca3(PO4)2), that are reinforced with silicate (basalt-based) fiberglass, is considered. The obtained materials were characterized by the XRD and SEM methods, mechanical compression tests were carried out, the setting times of cements were determined, changes in the pH of the aqueous medium in contact with the cements under study were measured. Microstructure analysis has been shown that the surface of the reinforcing fiber in contact with the matrix of hardening cement is partially corroded with the formation of phosphate microparticles on it. By pH-metry it was found that the samples during prolonged contact with water do not significantly change the pH value of the aquatic environment, which remains in the nearly neutral range from 5 to 7.5, favorable for further biological tests.\",\"PeriodicalId\":18298,\"journal\":{\"name\":\"Materials Science-medziagotyra\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.8000,\"publicationDate\":\"2023-02-21\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Science-medziagotyra\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.31044/1684-579x-2023-0-5-19-27\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Science-medziagotyra","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.31044/1684-579x-2023-0-5-19-27","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0

摘要

考虑了基于同构阳离子-(Na+,K+)和阴离子-(SiO44-,SO42-)取代的磷酸三钙(β和α-TCP,Ca3(PO4)2),用硅酸盐(玄武岩基)玻璃纤维增强的骨植入物反应硬化磷酸盐材料(磷酸盐水泥)的增强。通过XRD和SEM方法对所获得的材料进行了表征,进行了机械压缩试验,确定了水泥的凝结时间,测量了与所研究的水泥接触的水介质的pH值的变化。微观结构分析表明,与硬化水泥基体接触的增强纤维表面被部分腐蚀,并在其上形成磷酸盐微粒。通过pH测定发现,样品在长时间与水接触时,不会显著改变水环境的pH值,其保持在从5到7.5的几乎中性的范围内,有利于进一步的生物测试。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Calcium phosphate brushite cements made from substituted tricalcium phosphate Ca3(PO4)2 and reinforced with silicate glass fiber
The reinforcement of reaction hardening phosphate materials (phosphate cements) for bone implants, based on isomorphically cation- (Na+, K+) and anion- (SiO44-, SO42-) substituted tricalcium phosphate (β and α-TCP, Ca3(PO4)2), that are reinforced with silicate (basalt-based) fiberglass, is considered. The obtained materials were characterized by the XRD and SEM methods, mechanical compression tests were carried out, the setting times of cements were determined, changes in the pH of the aqueous medium in contact with the cements under study were measured. Microstructure analysis has been shown that the surface of the reinforcing fiber in contact with the matrix of hardening cement is partially corroded with the formation of phosphate microparticles on it. By pH-metry it was found that the samples during prolonged contact with water do not significantly change the pH value of the aquatic environment, which remains in the nearly neutral range from 5 to 7.5, favorable for further biological tests.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
Materials Science-medziagotyra
Materials Science-medziagotyra 工程技术-材料科学:综合
CiteScore
1.70
自引率
10.00%
发文量
92
审稿时长
6-12 weeks
期刊介绍: It covers the fields of materials science concerning with the traditional engineering materials as well as advanced materials and technologies aiming at the implementation and industry applications. The variety of materials under consideration, contributes to the cooperation of scientists working in applied physics, chemistry, materials science and different fields of engineering.
期刊最新文献
The Effect of Self-Healing Microorganism-Encapsulating Concrete on Enhancing Concrete Compressive Strength Fabrication of Functional Coating Layer for Emerging Transparent Electrodes using Antimony Tin Oxide Nano-colloid Fabrication of High-Performance Insulated Metal Substrates Employing h-BN Mixture/Epoxy Composite Coated on Roughened Copper Plate Performance and Phase Change Kinetic Investigations on Capric-Myristic Acid Eutectic Mixtures for Energy-Saving Construction The Photocatalytic Activity of the Bi2O3-B2O3-ZnO-TiO2 Glass Coating
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1