草酸盐沉淀水热法从电弧炉固体废物中生产ZnO

Lukman Nulhakim, I. Prasetyo, M. Rozana, W. Astuti
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引用次数: 0

摘要

电弧炉(EAF)废液含锌50-60%。电炉废渣合成具有生产氧化锌的潜力,可用于多种用途。采用水热法合成,时间变化为3和6小时,温度变化为120℃、150℃和200℃,沉淀剂为氢氧化钠(NaOH)和草酸(C2H2O4)。紫外可见分光光度计表征结果显示在365 nm处的吸光度值,这是ZnO材料的吸光度特性。XRF表征揭示了锌元素增加的结果。XRD表征表明草酸锌脱水。这一结果描述了以草酸为溶剂的水热脱水在不同温度和时间变化下制备草酸锌的过程。
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ZnO Production from EAF Solid Waste Using Hydrothermal Methods via Oxalate Precipitation
Electric Arc Furnace (EAF) waste contains 50-60% Zn. EAF waste synthesis has the potential to produce ZnO, which can be used in a variety of applications. The hydrothermal method is used in the synthesis, with time variations of 3 and 6 hours and temperature variations of 120 °C, 150 °C and 200 °C using precipitating reagents in the form of sodium hydroxide (NaOH) and oxalic acid (C2H2O4). UV-Vis spectrophotometer characterization result shows the absorbance value at 365 nm, which is the absorbance characteristic of ZnO material. The result of increasing the Zn element was revealed by XRF characterization. The XRD characterization revealed zinc oxalate dehydrates. This result depicts the hydrothermal with the oxalic acid solvent used to produce zinc oxalate dehydration at various temperatures and time variations.
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