棕榈油空果束废肥中有机碳元素测定的Walkley黑法试验验证

Eksergi Pub Date : 2022-08-10 DOI:10.31315/e.v19i3.7267
Wakhid Khoirul Umar, Fandika Agustiyar, A. Rahma
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引用次数: 0

摘要

:棕榈油加工产生的许多固体废物都是空的果串,但它们的利用仍然有限。油棕榈空果包(OPEFB)的用途之一是有机肥料。采用紫外-可见分光光度计对OPEFB废弃物中的有机肥料进行了有机碳法验证。本研究旨在验证有机碳在OPEFB肥料上的测试方法。OPEFB肥料中碳含量的测定参考分析群落协会(AOAC)的Walkley-Black方法。有机碳在OPEFB肥料上的测试结果表明,获得的相关系数(r)为100%,%RSD值为0.40%意味着该值低于4.72的2/3 CV Horwitz。准确度为106.99%。LOD为2.45,LOQ为8.17。因此,仪器的限值由LOD值2.49和LOQ值8.32得出;试验结果表明,符合验收条件。Walkley-Black法测定OPEFB肥料中有机碳的试验结果是有效的,该方法可用于OPEFB肥料有机碳含量的测定。
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Verification of the Walkley Black Method Test for Determination of Organic Carbon Elements in Palm Oil Empty Fruit Bunch Waste Fertilizer
: Many solid wastes from palm oil processing are empty fruit bunches, but their utilization is still limited. o ne of the uses of Oil Palm Empty Fruit Bunches ( OPEFB ) is organic fertilizer. The organic carbon method was verified on organic fertilizer from OPEFB waste using a UV-Vis Spectrophotometer. This study aims to verify the method of testing organic carbon on OPEFB fertilizer. Determination of carbon content in OPEFB fertilizer refers to the Association of Analytical Communities (AOAC) with the Walkley Black method. The results of the organic carbon test on OPEFB fertilizer show that the correlation coefficient (r) obtained is 100% , and the % RSD value of 0.40% means that the value is below 2/3 CV Horwitz of 4.72. accuracy with a value of 106.99%. The LOD is 2.45, and the LOQ is 8.17. Therefore, the limit value of the instrument is obtained by the LOD value of 2.49 and the LOQ of 8.32; the test results obtained indicate that it has complied with the conditions with acceptance. The test results for determining organic carbon in OPEFB fertilizer using the Walkley Black method showed valid results, so the method can be used to test organic carbon levels in OPEFB fertilizer.
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