麻风树花提取物介导的银纳米颗粒的绿色合成:光谱、催化和抗氧化分析

IF 16.4 1区 化学 Q1 CHEMISTRY, MULTIDISCIPLINARY Accounts of Chemical Research Pub Date : 2022-10-25 DOI:10.1080/00387010.2022.2137200
A. Bala, G. Rani, R. Ahlawat
{"title":"麻风树花提取物介导的银纳米颗粒的绿色合成:光谱、催化和抗氧化分析","authors":"A. Bala, G. Rani, R. Ahlawat","doi":"10.1080/00387010.2022.2137200","DOIUrl":null,"url":null,"abstract":"Abstract Plant extract mediated nanoparticles have gained enormous attention for their green and rational approach and developed as an alternative to conventional chemical and physical methods. Here, the less exploited Jatropha integerrima flower extract is used in the synthesis of silver nanoparticles. The as-prepared nanoparticles exhibit a strong surface plasma resonance around 420 nm. Several spectroscopic techniques confirmed the formation of silver nanoparticles with an average size of 32.07 nm, stabilized by functional groups. The catalytic activity of synthesized nanoparticles for Rhodamine B dye degradation in the presence of sodium borohydride was investigated. The results showed that the 100 µL catalyst dose degraded the alkaline solution of dye up to 98%, with a high rate constant of 1.2110 min−1. In addition, the nanoparticles were tested for antioxidant activity using the 2,2-dipehnyl-1-picrylhydrazyl free radical assay. The calculated IC50 value for synthesized nanoparticles was 33.63 ± 0.53 µg/mL. Thus, the as-prepared nanoparticles are excellent candidates for catalytic and antioxidant activities compared to other materials used so far.","PeriodicalId":1,"journal":{"name":"Accounts of Chemical Research","volume":null,"pages":null},"PeriodicalIF":16.4000,"publicationDate":"2022-10-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"Jatropha integerrima flower extract mediated green synthesis of silver nanoparticles: spectroscopic, catalytic, and antioxidant analysis\",\"authors\":\"A. Bala, G. Rani, R. Ahlawat\",\"doi\":\"10.1080/00387010.2022.2137200\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Abstract Plant extract mediated nanoparticles have gained enormous attention for their green and rational approach and developed as an alternative to conventional chemical and physical methods. Here, the less exploited Jatropha integerrima flower extract is used in the synthesis of silver nanoparticles. The as-prepared nanoparticles exhibit a strong surface plasma resonance around 420 nm. Several spectroscopic techniques confirmed the formation of silver nanoparticles with an average size of 32.07 nm, stabilized by functional groups. The catalytic activity of synthesized nanoparticles for Rhodamine B dye degradation in the presence of sodium borohydride was investigated. The results showed that the 100 µL catalyst dose degraded the alkaline solution of dye up to 98%, with a high rate constant of 1.2110 min−1. In addition, the nanoparticles were tested for antioxidant activity using the 2,2-dipehnyl-1-picrylhydrazyl free radical assay. The calculated IC50 value for synthesized nanoparticles was 33.63 ± 0.53 µg/mL. Thus, the as-prepared nanoparticles are excellent candidates for catalytic and antioxidant activities compared to other materials used so far.\",\"PeriodicalId\":1,\"journal\":{\"name\":\"Accounts of Chemical Research\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":16.4000,\"publicationDate\":\"2022-10-25\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Accounts of Chemical Research\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://doi.org/10.1080/00387010.2022.2137200\",\"RegionNum\":1,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"CHEMISTRY, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Accounts of Chemical Research","FirstCategoryId":"92","ListUrlMain":"https://doi.org/10.1080/00387010.2022.2137200","RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 3

摘要

摘要植物提取物介导的纳米颗粒以其绿色、合理的方法获得了广泛的关注,并作为传统化学和物理方法的替代品而发展起来。在这里,较少开发的麻疯树花提取物被用于合成银纳米粒子。制备的纳米颗粒在420 nm附近表现出强烈的表面等离子体共振。几种光谱技术证实了银纳米颗粒的形成,其平均尺寸为32.07 nm,由官能团稳定。研究了合成的纳米颗粒在硼氢化钠存在下对罗丹明B染料降解的催化活性。结果表明,100µL催化剂对染料碱性溶液的降解率可达98%,降解速率常数为1.2110 min−1。此外,采用2,2-二苯基-1-苦味酰肼自由基法检测纳米颗粒的抗氧化活性。合成纳米颗粒的IC50值为33.63±0.53µg/mL。因此,与目前使用的其他材料相比,制备的纳米颗粒具有良好的催化和抗氧化活性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Jatropha integerrima flower extract mediated green synthesis of silver nanoparticles: spectroscopic, catalytic, and antioxidant analysis
Abstract Plant extract mediated nanoparticles have gained enormous attention for their green and rational approach and developed as an alternative to conventional chemical and physical methods. Here, the less exploited Jatropha integerrima flower extract is used in the synthesis of silver nanoparticles. The as-prepared nanoparticles exhibit a strong surface plasma resonance around 420 nm. Several spectroscopic techniques confirmed the formation of silver nanoparticles with an average size of 32.07 nm, stabilized by functional groups. The catalytic activity of synthesized nanoparticles for Rhodamine B dye degradation in the presence of sodium borohydride was investigated. The results showed that the 100 µL catalyst dose degraded the alkaline solution of dye up to 98%, with a high rate constant of 1.2110 min−1. In addition, the nanoparticles were tested for antioxidant activity using the 2,2-dipehnyl-1-picrylhydrazyl free radical assay. The calculated IC50 value for synthesized nanoparticles was 33.63 ± 0.53 µg/mL. Thus, the as-prepared nanoparticles are excellent candidates for catalytic and antioxidant activities compared to other materials used so far.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
Accounts of Chemical Research
Accounts of Chemical Research 化学-化学综合
CiteScore
31.40
自引率
1.10%
发文量
312
审稿时长
2 months
期刊介绍: Accounts of Chemical Research presents short, concise and critical articles offering easy-to-read overviews of basic research and applications in all areas of chemistry and biochemistry. These short reviews focus on research from the author’s own laboratory and are designed to teach the reader about a research project. In addition, Accounts of Chemical Research publishes commentaries that give an informed opinion on a current research problem. Special Issues online are devoted to a single topic of unusual activity and significance. Accounts of Chemical Research replaces the traditional article abstract with an article "Conspectus." These entries synopsize the research affording the reader a closer look at the content and significance of an article. Through this provision of a more detailed description of the article contents, the Conspectus enhances the article's discoverability by search engines and the exposure for the research.
期刊最新文献
Mentorship in academic musculoskeletal radiology: perspectives from a junior faculty member. Underlying synovial sarcoma undiagnosed for more than 20 years in a patient with regional pain: a case report. Sacrococcygeal chordoma with spontaneous regression due to a large hemorrhagic component. Associations of cumulative voriconazole dose, treatment duration, and alkaline phosphatase with voriconazole-induced periostitis. Can the presence of SLAP-5 lesions be predicted by using the critical shoulder angle in traumatic anterior shoulder instability?
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1