国内各厂家甜奶油油的安全性、质量及造假判定

V. Lyasota, N. Bogatko, N. Bukalova, V. Dzhmil, O. Khitska, T. Mazur, S. Tkachuk, T. Prilipko, S. Giptenko
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The object of the study was the assessment of organoleptic, physicochemical, microbiological parameters and falsification of sweet butter obtained from various milk processing enterprises of Ukraine: Lustdorf LLC and Fooddevelopment LLC, Vinnytsia region; TDV \"Yagotinsky butter factory\"; PE \"SIMOL\", Kyiv region; State Enterprise \"Starokostiantyniv Dairy Plant\", Khmelnytsky region. Analytical, organoleptic (appearance, color, consistency, smell, taste) were used to achieve the research goal; physicochemical (mass fraction of moisture, mass fraction of fat, titrated acidity of plasma oil and acidity of fatty phase of oil, mass fraction of sodium chloride, determination of margarine and vegetable fats), microbiological (KMAFАNM, the presence of Escherichia coli bacteria, pathogenic microorganisms, in particular genus Salmonella, species Listeria monocytogenes; molds) and variation-statistical research methods. Developed patented express method for detecting adulteration of sweet cream oil using resorcinol solution in benzene with a mass fraction of 5.0% and concentrated hydrochloric acid can be used in production laboratories at milk and dairy products, supermarkets, wholesale bases, shops and public laboratories. in laboratories of veterinary and sanitary examination in agro-industrial markets. The oil produced by different manufacturers according to organoleptic parameters: appearance, color, texture, smell and taste met the requirements of DSTU 4399: 2005. According to physical and chemical parameters, the samples of sweet butter also met DSTU 4399: 2005, except for sample № 5 (SE \"Starokostiantyniv Dairy Plant\" of Khmelnytsky region), which showed an increase of + 0.6% by weight of sodium chloride. 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引用次数: 1

摘要

国内产品进入欧洲市场给乌克兰企业家带来了增加产量、确保安全、质量和竞争力的任务。本研究的目的是评估从国内各生产商获得的甜黄油的安全性和质量,并通过公认的方法和已开发的专利明示方法确定其伪造性。该研究的目的是评估从乌克兰的各种牛奶加工企业获得的甜黄油的感官、物理化学、微生物参数和伪造情况:Lustdorf LLC和Fooddevelopment LLC,Vinnytsia地区;TDV“Yagotinsky黄油厂”;PE“SIMOL”,基辅地区;国营企业“Starokostiantyniv乳品厂”,赫梅利尼茨基地区。分析、感官(外观、颜色、稠度、气味、味道)用于实现研究目标;物理化学(水分质量分数、脂肪质量分数、血浆油的滴定酸度和油的脂肪相酸度、氯化钠质量分数、人造黄油和植物脂肪的测定),微生物学(KMAFАNM,大肠杆菌的存在,病原微生物,特别是沙门氏菌属,单核细胞增多性李斯特菌属;霉菌)和变异统计研究方法。开发的专利快速检测甜奶油油掺假的方法,使用质量分数为5.0%的间苯二酚苯溶液和浓盐酸,可用于牛奶和乳制品生产实验室、超市、批发基地、商店和公共实验室。在农产品工业市场的兽医和卫生检查实验室。不同制造商根据感官参数生产的油:外观、颜色、质地、气味和味道符合DSTU 4399:2005的要求。根据理化参数,除样品外,甜黄油样品也符合DSTU 4399:2005№ 5(赫梅利尼茨基地区的SE“Starokostiantyniv奶牛场”),其显示氯化钠的重量增加了+0.6%。研究已经根据开发的专利方法建立了甜奶油油的伪造,根据该方法,指标中的概率为99.9%,生产:TDV“Yagotinsky黄油厂”-高达1.5%(浅紫色)油和“农场农民”,制造商LLC食品开发”-从1.6%到5.0%(亮紫色).甜黄油的微生物参数:KMAFANM,大肠杆菌属细菌,沙门氏菌属细菌,单核细胞增多性李斯特菌属细菌以及霉菌符合DSTU 4399:2005的要求。关键词:甜黄油,乌克兰乳制品加工企业,感官,理化,微生物指标,伪造,安全,质量。
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Safety and quality of sweet and cream oil of various domestic manufacturers and determining its falsification
The entry of domestic products into European markets has set Ukrainian entrepreneurs the task - to increase their production, ensure safety, quality and competitiveness. The purpose of the study is to assess the safety and quality of sweet butter obtained from various domestic producers, and to determine its falsification by the generally accepted method and the developed patented express method. The object of the study was the assessment of organoleptic, physicochemical, microbiological parameters and falsification of sweet butter obtained from various milk processing enterprises of Ukraine: Lustdorf LLC and Fooddevelopment LLC, Vinnytsia region; TDV "Yagotinsky butter factory"; PE "SIMOL", Kyiv region; State Enterprise "Starokostiantyniv Dairy Plant", Khmelnytsky region. Analytical, organoleptic (appearance, color, consistency, smell, taste) were used to achieve the research goal; physicochemical (mass fraction of moisture, mass fraction of fat, titrated acidity of plasma oil and acidity of fatty phase of oil, mass fraction of sodium chloride, determination of margarine and vegetable fats), microbiological (KMAFАNM, the presence of Escherichia coli bacteria, pathogenic microorganisms, in particular genus Salmonella, species Listeria monocytogenes; molds) and variation-statistical research methods. Developed patented express method for detecting adulteration of sweet cream oil using resorcinol solution in benzene with a mass fraction of 5.0% and concentrated hydrochloric acid can be used in production laboratories at milk and dairy products, supermarkets, wholesale bases, shops and public laboratories. in laboratories of veterinary and sanitary examination in agro-industrial markets. The oil produced by different manufacturers according to organoleptic parameters: appearance, color, texture, smell and taste met the requirements of DSTU 4399: 2005. According to physical and chemical parameters, the samples of sweet butter also met DSTU 4399: 2005, except for sample № 5 (SE "Starokostiantyniv Dairy Plant" of Khmelnytsky region), which showed an increase of + 0.6% by weight of sodium chloride. Research has established the falsification of sweet cream oil according to the developed patented method, according to which the probability in the indicators was 99.9%, produced: TDV "Yagotinsky butter factory" - up to 1.5% (light purple color) oil and "Farm Peasant", manufacturer LLC Food Development "- from 1.6 to 5.0% (bright purple color). Microbiological parameters of sweet butter: KMAFANM, bacteria of the Escherichia coli group, bacteria of the genus Salmonella, species Listeria monocytogenes, as well as molds met the requirements of DSTU 4399: 2005. Key words: sweet and butter, dairy processing enterprises of Ukraine, organoleptic, physicochemical, microbiological indicators, falsification, safety, quality.
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